Rojek Sebastian, Kłys Małgorzata, Scisłowski Mariusz
Katedry i Zakładu Medycyny Sadowej CM UJ.
Arch Med Sadowej Kryminol. 2005 Jul-Sep;55(3):195-205.
The Society of Hair Testing--SoHT organized a quality control test: "2004 Proficiency Test on Drugs of Abuse in Hair". 23 toxicological units participated in the test, among them the Toxicological Laboratory of The Institute of Forensic Medicine CM UJ. Five hair samples were obtained for analysis comprising four groups of drugs of abuse as follows: opioids (6-monoacethylmorphine, morphine, codeine), amphetamine (amphetamine, methamphetamine, 3,4-methylendioxyamphetamine--MDA, 3,4-methylendioxymethamphetamine--MDMA, 3,4-methylendioxyethylamphetamine--MDEA), cocaine and metabolites (benzoiloecgonine, cocaethylene) and cannabinoids (D9-tetrahydrocannabinol --9-THC, cannabinol--CBN). Obtained results were evaluated positively in all groups of drugs which were the subject of examination. Liquid chromatography coupled with tandem mass spectrometry in chemical ionization under atmospheric pressure option (LC-APCI-MS-MS) and gas chromatography coupled with tandem mass spectrometry and electron-impact ionization mode (GC-EI-MS-MS) were applied for analysis of analytes.
毛发检测协会（SoHT）组织了一次质量控制测试：“2004年毛发中滥用药物能力验证测试”。23个毒理学单位参与了此次测试，其中包括雅盖隆大学医学院法医学研究所毒理学实验室。共获取了5份毛发样本用于分析，这些样本包含以下四类滥用药物：阿片类药物（6-单乙酰吗啡、吗啡、可待因）、苯丙胺类（苯丙胺、甲基苯丙胺、3,4-亚甲基二氧基苯丙胺——MDA、3,4-亚甲基二氧基甲基苯丙胺——MDMA、3,4-亚甲基二氧基乙基苯丙胺——MDEA）、可卡因及其代谢物（苯甲酰爱康宁、可卡因乙烯酯）和大麻素类（Δ⁹-四氢大麻酚——9-THC、大麻酚——CBN）。在所有受检药物组中获得的结果均得到了肯定评价。采用大气压化学电离液相色谱-串联质谱法（LC-APCI-MS-MS）以及电子轰击电离模式的气相色谱-串联质谱法（GC-EI-MS-MS）对分析物进行分析。
