Lee In-Bog, Cho Byeong-Hoon, Son Ho-Hyun, Um Chung-Moon, Lim Bum-Soon
Department of Conservative Dentistry and Dental Research Institute, College of Dentistry, Seoul National University, 28-2 Yeongeon-Dong, Jongro-Ku, Seoul 110-749, South Korea.
Dent Mater. 2006 Nov;22(11):1071-9. doi: 10.1016/j.dental.2005.08.012. Epub 2005 Dec 20.
This study investigated the effect of the consistency, specimen geometry and adhesion on the measurements of axial polymerization shrinkage of light cured composite resins using an axial shrinkage-measuring device.
Four commercially available composites were examined: an anterior posterior hybrid composite Z100, a posterior packable composite P60 and two flowable composites, Filtek flow and Tetric flow. The axial polymerization shrinkage of the composites was determined using a 'bonded disc method' and 'non-bonded' free shrinkage method at varying C-factors by altering the specimen geometry. These measured axial shrinkages were compared with the free volumetric shrinkages. The consistency of the composites was also compared using a squeeze test.
Using the non-bonded method, the axial shrinkage was approximately one third of the true volumetric shrinkage as a result of isotropic contraction. However, in the bonded disc method, the axial shrinkage increased up to the volumetric shrinkage by anisotropic contraction as the bonded surface increased. The axial shrinkage increased with the increasing C-factor. It approached the true volumetric shrinkage and reached a plateau at near a C-factor of 5-6. However, in flowable composites, a lower level of axial shrinkage was measured by the compensational radial flow.
When estimating the volumetric shrinkage from the axial shrinkage measured using the bonded disc method, the C-factor of the specimen should be higher than 5 and the consistency of the composite is also an important factor that needs to be considered.
本研究使用轴向收缩测量装置,研究了光固化复合树脂的稠度、试样几何形状和附着力对轴向聚合收缩测量的影响。
检测了四种市售复合材料:一种前后牙通用混合型复合树脂Z100、一种后牙可压实复合树脂P60以及两种可流动复合树脂Filtek flow和Tetric flow。通过改变试样几何形状,在不同C因子下,使用“粘结圆盘法”和“非粘结”自由收缩法测定复合材料的轴向聚合收缩。将这些测得的轴向收缩与自由体积收缩进行比较。还使用挤压试验比较了复合材料的稠度。
使用非粘结法时,由于各向同性收缩,轴向收缩约为真实体积收缩的三分之一。然而,在粘结圆盘法中,随着粘结表面的增加,由于各向异性收缩,轴向收缩增加至体积收缩。轴向收缩随C因子的增加而增加。它接近真实体积收缩,并在C因子接近5 - 6时达到平稳状态。然而,在可流动复合树脂中,通过补偿径向流动测得的轴向收缩水平较低。
当使用粘结圆盘法从测得的轴向收缩估计体积收缩时,试样的C因子应高于5,并且复合材料的稠度也是需要考虑的一个重要因素。