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视频原子力显微镜——一种用于高速表面分析的新工具。

VideoAFM--a new tool for high speed surface analysis.

作者信息

Hobbs Jamie K, Vasilev Cvetelin, Humphris Andrew D L

机构信息

Department of Chemistry, University of Sheffield, Brook Hill, Sheffield S3 7HF, UK.

出版信息

Analyst. 2006 Feb;131(2):251-6. doi: 10.1039/b511330j. Epub 2005 Nov 11.

Abstract

The VideoAFM provides a 1000 fold increase in image rate compared to conventional atomic force microscopes, giving nanometre resolution images of surfaces at a rate of 15 frames s(-1), which is approximately 1 million pixels s(-1). Images of high stiffness surfaces such as calibration grids are provided for the first time, and allow for a more rigorous examination of the meaning of the data obtained with the VideoAFM. Instrumental changes that could provide true topographic images are discussed. The advantages of a high speed scanning technique that is integrated within a conventional AFM are outlined. Particular emphasis is given to the capability to 'tile' images, and hence rapidly map large areas with nanometre resolution. It is found that the inherent increase in stability that comes from a high frame rate leads to the possibility of manually manipulating the sample while maintaining a sharp image, allowing real-time user interaction with the AFM. The possible application of the VideoAFM approach for the very rapid analysis of surface properties and, ultimately, surface chemistry is discussed and some possible routes are given.

摘要

与传统原子力显微镜相比,视频原子力显微镜的成像速率提高了1000倍,能够以15帧/秒(即约100万像素/秒)的速率提供表面的纳米级分辨率图像。首次提供了诸如校准网格等高刚度表面的图像,这使得能够更严格地检验通过视频原子力显微镜获得的数据的意义。讨论了能够提供真实形貌图像的仪器改进。概述了集成在传统原子力显微镜内的高速扫描技术的优点。特别强调了“拼接”图像的能力,从而能够以纳米分辨率快速绘制大面积区域。研究发现,高帧率带来的稳定性固有提高使得在保持清晰图像的同时手动操作样品成为可能,从而实现用户与原子力显微镜的实时交互。讨论了视频原子力显微镜方法在非常快速地分析表面性质以及最终分析表面化学方面的可能应用,并给出了一些可能的途径。

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