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用于同步辐射硬X射线微束原位实验的扫描隧道显微镜的研制。

Development of a scanning tunneling microscope for in situ experiments with a synchrotron radiation hard-X-ray microbeam.

作者信息

Saito Akira, Maruyama Junpei, Manabe Ken, Kitamoto Katsuyuki, Takahashi Koji, Takami Kazuhiro, Yabashi Makina, Tanaka Yoshihito, Miwa Daigo, Ishii Masashi, Takagi Yasumasa, Akai-Kasaya Megumi, Shin Shik, Ishikawa Tetsuya, Kuwahara Yuji, Aono Masakazu

机构信息

Department of Material and Life Science, Osaka University, Osaka 565-0871, Japan.

出版信息

J Synchrotron Radiat. 2006 Mar;13(Pt 2):216-20. doi: 10.1107/S0909049506001622. Epub 2006 Feb 17.

Abstract

A scanning tunneling microscope dedicated to in situ experiments under the irradiation of highly brilliant hard-X-rays of synchrotron radiation has been developed. In situ scanning tunneling microscopy (STM) observation was enabled by developing an accurate alignment system in ultrahigh vacuum. Despite the noisy conditions of the synchrotron radiation facility and the radiation load around the probe tip, STM images were successfully obtained at atomic resolution. Tip-current spectra were obtained for Ge nano-islands on a clean Si(111) surface by changing the incident photon energy across the Ge absorption edge. A current modification was detected at the absorption edge with a spatial resolution of the order of 10 nm.

摘要

已开发出一种用于在同步辐射的高亮度硬X射线照射下进行原位实验的扫描隧道显微镜。通过在超高真空环境中开发精确的对准系统,实现了原位扫描隧道显微镜(STM)观察。尽管同步辐射设施存在噪声条件以及探针尖端周围存在辐射负载,但仍成功获得了原子分辨率的STM图像。通过在锗吸收边缘改变入射光子能量,获得了清洁Si(111)表面上锗纳米岛的尖端电流谱。在吸收边缘检测到电流变化,其空间分辨率约为10纳米。

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