Zhao Ai-dong, Zhai Xue-liang, Liu Jing-ze
Experiment Centre, Hebei Nomal University, Shijiazhuang 050016, China.
Guang Pu Xue Yu Guang Pu Fen Xi. 2005 Nov;25(11):1893-4.
In the present paper, microwave digestion technique was used to determine Ca, Zn, Cu, Mg and Fe in rat liver by flame atomic absorption spectrometry (FAAS). The effect of microwave digestion condition on the analysis results was examined and the best analysis condition of FAAS was selected. Compared to traditional wet methods, the experimental result showed that the method is rapid, sample digestion is complete, the blank value is low, and the measurement result is satisfactory. Applied to the determination of trace elements in rat liver, the method proved to be selective with satisfactory recovery of 96%-103% andrelative standard deviation of 1.0%-2.6%.
本文采用微波消解技术,通过火焰原子吸收光谱法(FAAS)测定大鼠肝脏中的钙、锌、铜、镁和铁。考察了微波消解条件对分析结果的影响,选择了FAAS的最佳分析条件。与传统湿法相比,实验结果表明该方法快速、样品消解完全、空白值低,测量结果令人满意。该方法用于大鼠肝脏中微量元素的测定,具有良好的选择性,回收率为96%-103%,相对标准偏差为1.0%-2.6%,结果令人满意。