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用于增强钛与瓷结合的钛表面Cr-Ti-Al-N复合涂层

[Cr-Ti-Al-N complex coating on titanium to strengthen Ti/porcelain bonding].

作者信息

Zhang Hui, Guo Tian-wen, Li Jun-ming, Pan Jing-guang, Dang Yong-gang, Tong Yu

机构信息

Department of Prosthodontics, School of Stomatology, Fourth Military Medical University, Xi'an 710032, China.

出版信息

Nan Fang Yi Ke Da Xue Xue Bao. 2006 Feb;26(2):154-7.

Abstract

OBJECTIVE

To study the feasibility of magnetron sputtering Cr-Ti-Al-N complex coating as an interlayer on titanium to enhance the titanium-ceramic binding strength.

METHODS

With a three-point bending test according to ISO 9693, the binding strength of Duceratin (Degussa) to titanium substrate prepared with 4 different surface treatments (polishing, polishing and megnetron sputtering Cr, Ti, Al, and N complex coating, sandblasting, sandblasting and coating) was evaluated. Ti/porcelain interface and fractured Ti surface were examined using scanning electron microscopy with energy-dispersive spectrometry (EDS).

RESULTS

The binding strength of polished and coated titanium/Duceratin was significantly higher than polished titanium group (P<0.05). The binding strength of sandblasted and coated titanium/Duceratin did not differ significantly from that of sandblasted titanium group (P>0.05), and the strength in the two sandblasted titanium groups was significantly higher than that in polished and coated titanium group (P<0.05).

CONCLUSION

Megnetron sputtering Cr-Ti-Al-N complex on polished titanium can increase the titanium/porcelain binding strength. Megnetron sputtering coating is a promising Ti/porcelain interlayer.

摘要

目的

研究磁控溅射Cr-Ti-Al-N复合涂层作为钛表面中间层以提高钛-陶瓷结合强度的可行性。

方法

根据ISO 9693进行三点弯曲试验,评估Duceratin(德固赛)与经过4种不同表面处理(抛光、抛光并磁控溅射Cr、Ti、Al和N复合涂层、喷砂、喷砂并涂层)制备的钛基底之间的结合强度。使用带有能谱仪(EDS)的扫描电子显微镜检查Ti/瓷界面和断裂的Ti表面。

结果

抛光并涂层的钛/Duceratin的结合强度显著高于抛光钛组(P<0.05)。喷砂并涂层的钛/Duceratin的结合强度与喷砂钛组无显著差异(P>0.05),且两个喷砂钛组的强度显著高于抛光并涂层的钛组(P<0.05)。

结论

在抛光钛上磁控溅射Cr-Ti-Al-N复合物可提高钛/瓷结合强度。磁控溅射涂层是一种有前景的Ti/瓷中间层。

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