Raghothamachar Balaji, Dhanaraj Govindhan, Bai Jie, Dudley Michael
Department of Materials Science and Engineering, SUNY at Stony Brook, Stony Brook, New York 11794-2275, USA.
Microsc Res Tech. 2006 May;69(5):343-58. doi: 10.1002/jemt.20290.
A brief review of X-ray topography--a nondestructive method for direct observation and characterization of defects in single crystals--is presented here. The origin and development of this characterization method and the different techniques derived from it are described. Emphasis is placed on synchrotron X-ray topography and its application in studying various crystal imperfections. Mechanisms of contrast formation on X-ray topographs are discussed, with emphasis on contrast associated with dislocations. Determination of Burgers vectors and line directions of dislocations from analysis of X-ray topographs is explained. Contrast from inclusions is illustrated, and their differentiation from dislocations is demonstrated with the aid of simulated topographs. Contrast arising from the deformation fields associated with cracks is also briefly covered.
本文简要回顾了X射线形貌术——一种用于直接观察和表征单晶缺陷的无损方法。描述了这种表征方法的起源和发展以及由此衍生出的不同技术。重点介绍了同步辐射X射线形貌术及其在研究各种晶体缺陷中的应用。讨论了X射线形貌图上衬度形成的机制,重点是与位错相关的衬度。解释了通过分析X射线形貌图确定位错的伯格斯矢量和线方向。举例说明了夹杂物产生的衬度,并借助模拟形貌图展示了夹杂物与位错的区分。还简要介绍了与裂纹相关的变形场产生的衬度。