微波辅助由芳烃和α,β-不饱和酰氯一锅法合成1-茚酮。
Microwave-assisted one-pot synthesis of 1-indanones from arenes and alpha,beta-unsaturated acyl chlorides.
作者信息
Yin Wei, Ma Yuan, Xu Jiaxi, Zhao Yufen
机构信息
Key Laboratory of Bioorganic Phosphorus Chemistry and Chemical Biology, Ministry of Education, Department of Chemistry, Tsinghua University, Beijing 100084, People's Republic of China.
出版信息
J Org Chem. 2006 May 26;71(11):4312-5. doi: 10.1021/jo060022p.
PMID:16709078
Abstract
A series of 1-indanones were synthesized in good yields via tandem Friedel-Crafts acylation and Nazarov cyclization of arenes and alpha,beta-unsaturated acyl chlorides in the presence of aluminum chloride under microwave irradiation.
摘要
在微波辐射下，以氯化铝为催化剂，通过芳烃与α,β-不饱和酰氯的串联傅克酰基化反应和纳扎罗夫环化反应，高产率地合成了一系列1-茚酮。
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