[虎舌红根的化学成分]

[Chemical constituents from roots of Ardisia punctata].

作者信息

Li Chun, Yue Dang-Kun, Bu Peng-Bin, Sun You-Fu

机构信息

Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China.

出版信息

Zhongguo Zhong Yao Za Zhi. 2006 Apr;31(7):562-5.

PMID:16780159

Abstract

OBJECTIVE

To study the chemical constituents from the roots of Ardisia punctata.

METHOD

Compounds were isolated by chromatographic techniques on silica gel and Rp-HPLC column. Their structures were elucidated by chemical and spectroscopic methods.

RESULT

Twelve compounds were identified as 3-hydroxy-5-tridecyl-methyl phenyl ether (1), 5-pentadecyl-1, 3-benzenediol (2), 2-methoxy-6-tridecyl-1, 4-benzoquinone (3), 2-methoxy-6-pentadecyl-1, 4-benzoquinone (4), glutinol (5), ardisicrenoside A (6), ardisiacrispin B (7), 24-ethyl-5a-cholesta-7, 22(E)-dien-3-one (8), 24-ethyl-5alpha-cholesta-7, 22(E)-dien-3beta-ol (9), daucosterol (10), vanillin acid (11), tetratriacontanoic acid (12).

CONCLUSION

All the compounds were obtained from this plant for the first time.

摘要

目的

研究虎舌红根的化学成分。

方法

采用硅胶柱色谱和反相高效液相色谱柱色谱技术分离化合物，通过化学和光谱方法鉴定其结构。

结果

鉴定出12个化合物，分别为3-羟基-5-十三烷基甲基苯基醚（1）、5-十五烷基-1,3-苯二酚（2）、2-甲氧基-6-十三烷基-1,4-苯醌（3）、2-甲氧基-6-十五烷基-1,4-苯醌（4）、谷甾醇（5）、虎舌红苷A（6）、虎舌红素B（7）、24-乙基-5α-胆甾-7,22（E）-二烯-3-酮（8）、24-乙基-5α-胆甾-7,22（E）-二烯-3β-醇（9）、胡萝卜苷（10）、香草酸（11）、三十四烷酸（12）。