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采用共固化技术时复合树脂与自凝玻璃离子水门汀之间的粘结强度。

Bond strengths between composite resin and auto cure glass ionomer cement using the co-cure technique.

作者信息

Knight G M, McIntyre J M

机构信息

Dental School, Faculty of Health Sciences, The University of Adelaide, South Australia.

出版信息

Aust Dent J. 2006 Jun;51(2):175-9. doi: 10.1111/j.1834-7819.2006.tb00423.x.

Abstract

BACKGROUND

The clinical technique for sandwich restorations prescribes etching initially set auto cure glass ionomer cement (GIC) prior to placing a layer of resin bond to develop a weak mechanical bond between composite resin and GIC. Co-curing a resin modified glass ionomer cement (RMGIC) bond and composite resin to GIC may create a chemical bond and improve the bond strengths between these two materials.

METHODS

A total of 48 specimens were prepared, 12 in each of four categories. Capsulated GIC was placed into a mould and allowed to set for four minutes, etched for five seconds followed by placement of a resin bond and photo cured for five seconds over which a composite resin was puddled onto the resin bond and photo cured for 10 seconds. Capsulated GIC was placed into a mould and allowed to set for four minutes after which a sample of RMGIC (Riva LC) was prepared using twice the liquid powder ratio and painted over the surface of the set GIC using a micro brush. An increment of composite resin was added over the RMGIC and both materials were photo co-cured for 10 seconds. Capsulated GIC was placed into a mould and RMGIC (Riva LC) that had been prepared using twice the liquid powder was brushed over the GIC (prior to initial set) followed by the placement of a layer of composite resin and photo co-cured for 10 seconds. Capsulated GIC was placed into a mould and RMGIC (Fuji II LC) that had been prepared using twice the liquid powder was brushed over the GIC (prior to initial set) followed by the placement of a layer of composite resin and photo co-cured for 10 seconds. Shear testing of each of the samples was carried out and specimens were examined to determine the nature of the fracture. Selected samples were prepared for SEM investigation to observe the interfaces between the GIC and composite resin.

RESULTS

There were significantly lower bond strengths (P < 0.05) amongst samples that had been etched and bonded (2.42MPa) compared to the other samples that had been co-cure bonded with RMGIC (6.48-7.05MPa). There were no significant differences amongst the bond strengths of the samples co-cure bonded with RMGIC. Specimens prepared by the 'etch and bond' technique failed adhesively and co-cured specimens failed cohesively within the GIC. SEM investigation showed chemical bonds between RMGIC bond and GIC and composite resin.

CONCLUSIONS

The co-cured RMGIC bonding system eliminates several placement steps and produces a significantly stronger chemical bond between GIC and composite resin than the 'etch and bond' technique. RMGIC bond and composite resin may be co-cured to GIC either before or after initial set has occurred.

摘要

背景

三明治修复体的临床技术要求在放置一层树脂粘结剂之前,先蚀刻初始凝固的自凝玻璃离子水门汀(GIC),以在复合树脂和GIC之间形成较弱的机械粘结。将树脂改性玻璃离子水门汀(RMGIC)粘结剂与复合树脂和GIC共同固化可能会形成化学键,并提高这两种材料之间的粘结强度。

方法

共制备48个样本,分为四类,每类12个。将胶囊装的GIC放入模具中,静置4分钟,蚀刻5秒,然后放置树脂粘结剂并光固化5秒,在其上倒入复合树脂并光固化10秒。将胶囊装的GIC放入模具中,静置4分钟,然后使用两倍液粉比制备RMGIC(丽娃LC)样本,并用微型刷子涂覆在凝固的GIC表面。在RMGIC上添加一层复合树脂,两种材料共同光固化10秒。将胶囊装的GIC放入模具中,将使用两倍液粉比制备的RMGIC(丽娃LC)在GIC(初始凝固前)上刷涂,然后放置一层复合树脂并光固化10秒。将胶囊装的GIC放入模具中,将使用两倍液粉比制备的RMGIC(富士II LC)在GIC(初始凝固前)上刷涂,然后放置一层复合树脂并光固化10秒。对每个样本进行剪切测试,并检查样本以确定断裂的性质。选择样本进行扫描电子显微镜(SEM)研究,以观察GIC与复合树脂之间的界面。

结果

与其他用RMGIC共同固化粘结的样本(6.48 - 7.05MPa)相比,蚀刻并粘结的样本(2.42MPa)的粘结强度显著较低(P < 0.05)。用RMGIC共同固化粘结的样本的粘结强度之间没有显著差异。通过“蚀刻并粘结”技术制备的样本发生粘结性失效,共同固化的样本在GIC内发生内聚性失效。SEM研究显示RMGIC粘结剂与GIC和复合树脂之间存在化学键。

结论

共同固化的RMGIC粘结系统省去了几个放置步骤,并且与“蚀刻并粘结”技术相比,在GIC和复合树脂之间产生了显著更强的化学键。RMGIC粘结剂和复合树脂可以在初始凝固之前或之后与GIC共同固化。

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