一种用于磷酸盐化合物核磁共振表征的新型¹⁷O同位素富集方法。
A new 17O-isotopic enrichment method for the NMR characterisation of phosphate compounds.
作者信息
Flambard Alexandrine, Montagne Lionel, Delevoye Laurent
机构信息
UCCS, Unité de Catalyse et Chimie du Solide, UMR-CNRS 8181, Ecole Nationale Supérieure de Chimie de Lille, Université des Sciences et Technologies de Lille, BP90108, 59655 Villeneuve d'Ascq, France.
出版信息
Chem Commun (Camb). 2006 Aug 28(32):3426-8. doi: 10.1039/b604803j. Epub 2006 Jul 6.
DOI:10.1039/b604803j
PMID:16896483
Abstract
Heating phosphate compounds under (17)O-enriched water vapour is an easy and rapid method to prepare homogeneously enriched and pure samples for the acquisition of (17)O NMR spectra with a good sensitivity.
摘要
在富含¹⁷O的水蒸气中加热磷酸盐化合物是一种简便快速的方法，可制备均匀富集且纯净的样品，用于采集具有良好灵敏度的¹⁷O核磁共振谱。
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