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顶空-固相微萃取-气相色谱法测定水和城市废水中的氯化挥发性有机化合物

Determination of chlorinated volatile organic compounds in water and municipal wastewater using headspace-solid phase microextraction-gas chromatography.

作者信息

Antoniou Chrysoula V, Koukouraki Elisavet E, Diamadopoulos Evan

机构信息

Laboratory of Environmental Engineering and Management, Department of Environmental Engineering, Technical University of Crete, 73100 Chania, Greece.

出版信息

J Chromatogr A. 2006 Nov 3;1132(1-2):310-4. doi: 10.1016/j.chroma.2006.08.082. Epub 2006 Sep 26.

DOI:10.1016/j.chroma.2006.08.082
PMID:16999972
Abstract

The aim of this work was to develop a fast and simple analytical method for the determination of 14 chlorinated volatile organic compounds (VOCs) in water and wastewater samples. Headspace-solid-phase microextraction (HS-SPME) and gas chromatography (GC) were used for the determination of the VOCs. The extraction parameters were investigated in order to optimize the HS-SPME-GC method. The quality parameters of the method were also investigated.

摘要

这项工作的目的是开发一种快速简便的分析方法,用于测定水和废水样品中的14种挥发性有机氯化合物(VOCs)。采用顶空固相微萃取(HS-SPME)和气相色谱(GC)法测定VOCs。研究了萃取参数以优化HS-SPME-GC方法,还对该方法的质量参数进行了研究。

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