Wang X Y, Yap Adrian U J, Ngo H C, Chung S M
Department of Cariology, Endodontology and Operative Dentistry, Peking University School and Hospital of Stomatology, People's Republic of China.
J Biomed Mater Res B Appl Biomater. 2007 Jul;82(1):1-6. doi: 10.1002/jbm.b.30697.
This study investigated the effects of various environmental conditions on the hardness and elastic modulus of restorative glass-ionomer cements (GICs). Two resin-modified GICs (RMGICs) (Fuji II LC [FL]; Photac-Fil Quick [PQ]) and three highly viscous GICs (HVGICs) (Fuji IX Fast [FN]; KetacMolar [KM]; KetacMolar Quick [KQ]) were evaluated in this study. Specimens were fabricated according to the manufacturers' instructions and stored under a variety of conditions (n = 7): 100% humidity, distilled water, pH 5 demineralization solution, and pH 7 remineralization solution. The hardness and elastic modulus were measured using a depth-sensing microindentation test after 4 weeks. The results were analyzed using the independent samples T-test and ANOVA/Scheffe's post hoc test (p < 0.05). HVGICs showed significantly higher hardness and elastic modulus than RMGICs under all storage conditions. Storage in distilled water significantly increased the hardness and elastic modulus of FN, but decreased that of PQ. All HVGICs and RMGICs stored in remineralization solution had hardness values and elastic moduli comparable to those stored in water. Compared to remineralization solution, demineralization solution had no significant effects on the modified GICs with the exception of KQ. The results suggest that the mechanical properties of glass-ionomer restoratives are material-type and storage condition dependent. Therefore, the clinical selection of a glass-ionomer material should be based on the oral environment to which it will be subjected.
本研究调查了各种环境条件对修复用玻璃离子水门汀(GIC)硬度和弹性模量的影响。本研究评估了两种树脂改性GIC(RMGIC)(富士II LC [FL];光固化流体玻璃离子水门汀[PQ])和三种高粘性GIC(HVGIC)(富士IX快速型[FN];化学固化玻璃离子水门汀[KM];化学固化快速型玻璃离子水门汀[KQ])。根据制造商的说明制备样本,并在多种条件下(n = 7)储存:100%湿度、蒸馏水、pH 5脱矿溶液和pH 7再矿化溶液。4周后使用深度传感微压痕试验测量硬度和弹性模量。使用独立样本T检验和方差分析/谢费事后检验(p < 0.05)对结果进行分析。在所有储存条件下,HVGIC的硬度和弹性模量均显著高于RMGIC。储存在蒸馏水中显著提高了FN的硬度和弹性模量,但降低了PQ的硬度和弹性模量。所有储存在再矿化溶液中的HVGIC和RMGIC的硬度值和弹性模量与储存在水中的相当。与再矿化溶液相比,除KQ外,脱矿溶液对改性GIC没有显著影响。结果表明,玻璃离子修复材料的力学性能取决于材料类型和储存条件。因此,玻璃离子材料的临床选择应基于其所处的口腔环境。