Kostka A, Mälzer G, Eggeler G
Institut für Werkstoffe, Ruhr-Universität Bochum, 44780 Bochum, Germany.
J Microsc. 2006 Sep;223(Pt 3):295-7. doi: 10.1111/j.1365-2818.2006.01659.x.
The evolution of the dislocation structure that forms during uniaxial creep deformation in the single-crystal superalloy LEK94 of low density and with Re additions was analysed using transmission electron microscopy. The material has a gamma/gamma'-microstructure consisting of gamma'-cubes (L12 phase, 80 vol.%) separated by thin gamma-channels (face-centred cubic). <100> tensile creep tests were performed at 980 and 1020 degrees C at stresses of 200 and 240 MPa. The microstructure was investigated at three characteristic stages of creep (directly after loading, at 5% strain and after rupture) to show the evolution of the dislocation structure during high-temperature creep. It was found that in the early stages of creep, a(0)/2<011> dislocations form within the gamma-channels. Later on, dislocation networks form and gamma' cutting processes with a(0)/<001> superdislocations are observed. The results are in line with observations made for other superalloy single crystals in the high-temperature low-stress creep regime.
利用透射电子显微镜分析了低密度且添加铼的单晶高温合金LEK94在单轴蠕变变形过程中形成的位错结构的演变。该材料具有γ/γ'微观结构,由薄的γ通道(面心立方)分隔的γ'立方(L12相,80体积%)组成。在980和1020℃下,在200和240MPa的应力下进行了<100>拉伸蠕变试验。在蠕变的三个特征阶段(加载后立即、5%应变时和断裂后)对微观结构进行了研究,以显示高温蠕变过程中位错结构的演变。结果发现,在蠕变早期,γ通道内形成a(0)/2<011>位错。随后,形成位错网络,并观察到a(0)/<001>超位错的γ'切割过程。这些结果与在高温低应力蠕变状态下对其他单晶高温合金的观察结果一致。