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库尔勒香梨(Pyrus serotina Reld)贮藏期间挥发性成分及理化性质的变化

Changes in the volatile compounds and chemical and physical properties of Kuerle fragrant pear (Pyrus serotina Reld) during storage.

作者信息

Chen Ji Luan, Wu Ji Hong, Wang Qiang, Deng Hui, Hu Xiao Song

机构信息

Food College, Shihezi University, Xinjiang, China, 832003.

出版信息

J Agric Food Chem. 2006 Nov 15;54(23):8842-7. doi: 10.1021/jf061089g.

Abstract

Volatiles from stored Kuerle fragrant pears (Pyrus serotina Reld) were studied using high-resolution gas chromatography and the solid-phase microextraction (SPME) method of gas chromatography/mass spectrometry (GC/MS). The dominant components were hexanal, ethyl hexanoate, ethyl butanoate, ethyl acetate, hexyl acetate, ethanol, alpha-farnesene, butyl acetate, and ethyl (E,Z)-2,4-decadienoate. By using GC-olfactometry, it demonstrated that the volatile compounds from SPME were responsible for the aroma of the Kuerle fragrant pear. The levels of sugars, organic acids, and phenolic acids in Kuerle fragrant pears were investigated using high-performance liquid chromatography (HPLC). Fructose was the dominant sugar, followed by glucose and sucrose. With increasing storage time, sucrose levels decreased; however, changes in fructose and glucose levels were not remarkable. There was a slight decrease in flesh firmness during storage. The general soluble solids concentration (SSC) declined slightly after 5 months storage. Some aroma-related volatile components increased during storage, while others decreased, especially the esters. The organic acids and phenolic acids also changed. The flavor of the Kuerle fragrant pears was affected by the change of volatile compounds and changes in chemical and physical properties.

摘要

采用高分辨率气相色谱法和气相色谱/质谱联用(GC/MS)的固相微萃取(SPME)方法,对储存的库尔勒香梨(Pyrus serotina Reld)中的挥发性成分进行了研究。主要成分有己醛、己酸乙酯、丁酸乙酯、乙酸乙酯、乙酸己酯、乙醇、α-法尼烯、乙酸丁酯和(E,Z)-2,4-癸二烯酸乙酯。通过气相色谱-嗅觉测定法表明,固相微萃取得到的挥发性化合物构成了库尔勒香梨的香气。采用高效液相色谱法(HPLC)对库尔勒香梨中的糖、有机酸和酚酸含量进行了测定。果糖是主要糖类,其次是葡萄糖和蔗糖。随着储存时间的延长,蔗糖含量下降;然而,果糖和葡萄糖含量的变化并不显著。储存期间果肉硬度略有下降。储存5个月后,一般可溶性固形物浓度(SSC)略有下降。一些与香气相关的挥发性成分在储存期间增加,而另一些则减少,尤其是酯类。有机酸和酚酸也发生了变化。库尔勒香梨的风味受到挥发性化合物变化以及化学和物理性质变化的影响。

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