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[均相沉淀法制备CeO₂纳米晶的研究]

[The research on preparing CeO2 nanocrystalline by homogeneous precipitation method].

作者信息

Li Xia, Li Li

机构信息

College of Chemical and Environmental Science, Inner Mongolia Normal University, Huhhot 010022, China.

出版信息

Guang Pu Xue Yu Guang Pu Fen Xi. 2006 Sep;26(9):1746-8.

Abstract

CeO2 nanocrystallines were prepared by homogeneous complexed-precipitation method, using cerous nitrate and ammonium tartrate as raw materials. The effects of cerous tartrate complex compound and the way of producing precipitation on the particle size of samples were investigated. The samples were characterized by XRD, TEM and SEM. The SEM micrograph shows that the foam exhibits a perforated porousness stereostructure in shape, and the HRTEM picture of the particles reveals the clear crystal lattice. All the results indicate that the samples were CeO2 nanocrystalline.

摘要

采用硝酸铈和酒石酸铵为原料,通过均匀络合沉淀法制备了CeO₂纳米晶。研究了酒石酸铈络合物和沉淀方式对样品粒径的影响。采用XRD、TEM和SEM对样品进行了表征。SEM显微照片显示泡沫呈现出穿孔多孔立体结构,颗粒的HRTEM图像显示出清晰的晶格。所有结果表明样品为CeO₂纳米晶。

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