Bélanger Jacqueline M R, Paré J R Jocelyn, Turpin Rodney, Schaefer Joe, Chuang C W
Environment Canada, Green Technologies Division, 335 River Road, Ottawa, Ont., Canada K1A 0H3.
J Hazard Mater. 2007 Jun 25;145(1-2):336-8. doi: 10.1016/j.jhazmat.2006.12.074. Epub 2007 Jan 8.
The use of microwave energy as a heating source for the field-based headspace sampling and the subsequent determination of various volatile organic compounds (VOCs) using a field-portable HAPSITE gas chromatograph-mass spectrometer has been evaluated. A significant advantage in time reduction has been observed when using microwave energy when compared to conventional resistive-based heating. Such time savings are critical in field operations involving equipment such as the HAPSITE where non-routine sampling is commonly performed and very quick turnaround time is usually needed. Further, the technology also showed significant improvements in terms of sensitivity, thus suggesting its applicability to a broader range of compounds and detection levels than current technologies.
已对将微波能量用作基于现场的顶空采样的加热源,并随后使用现场便携式HAPSITE气相色谱-质谱仪测定各种挥发性有机化合物(VOC)进行了评估。与传统的电阻式加热相比,使用微波能量时在时间减少方面具有显著优势。在涉及HAPSITE等设备的现场操作中,这种时间节省至关重要,因为在这些操作中通常进行非常规采样,并且通常需要非常短的周转时间。此外,该技术在灵敏度方面也有显著提高,因此表明其比当前技术适用于更广泛的化合物和检测水平。