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6-羟基和1-甲基-6-羟基双环[2.2.2]辛烷-2-酮乙二醇缩醛及乙二醇二硫缩醛的光谱表征

Spectroscopic characterization of 6-hydroxy and 1-methyl-6-hydroxybicyclo[2.2.2]octan-2-one ethylene acetals and ethylene dithioacetals.

作者信息

Leonelli Francesca, Garofalo Barbara, La Bella Angela, Lasta Ermanno, Ceccacci Francesca, Migneco Luisa M, Marini Bettolo Rinaldo

机构信息

Istituto di Chimica Biomolecolare del CNR, Sezione di Roma, and Dipartimento di Chimica Università degli Studi di Roma La Sapienza, Piazzalle Aldo Moro 5, ROMA 62, I-00185 Rome, Italy.

出版信息

Magn Reson Chem. 2007 May;45(5):420-3. doi: 10.1002/mrc.1964.

DOI:10.1002/mrc.1964

PMID:17323384

Abstract

6-endo- and 6-exo-Hydroxybicyclo[2.2.2]octan-2-one and 1-methyl-6-endo- and 6-exo-hydroxybicyclo[2.2.2]octan-2-one ethylene acetals and ethylene dithioacetals 1-4 have been characterized by 1D and 2D NMR methods.

摘要

6-内型和6-外型-羟基双环[2.2.2]辛烷-2-酮以及1-甲基-6-内型和6-外型-羟基双环[2.2.2]辛烷-2-酮的亚乙基缩醛和亚乙基二硫缩醛1-4已通过一维和二维核磁共振方法进行了表征。