Azevedo Andrea, Machado Ana Lucia, Giampaolo Eunice Teresinha, Pavarina Ana Claudia, Vergani Carlos Eduardo
Department of Dental Materials and Prosthodontics, Araquara Dental School, UNESP - São Paulo State University, Araraquara, São Paulo, Brazil.
J Prosthodont. 2007 Jul-Aug;16(4):255-62. doi: 10.1111/j.1532-849X.2007.00188.x. Epub 2007 Apr 23.
The effect of water immersion on the shear bond strength (SBS) between 1 heat-polymerizing acrylic resin (Lucitone 550-L) and 4 autopolymerizing reline resins (Kooliner-K, New Truliner-N, Tokuso Rebase Fast-T, Ufi Gel Hard-U) was investigated. Specimens relined with resin L were also evaluated.
One hundred sixty cylinders (20 x 20 mm) of L denture base resin were processed, and the reline resins were packed on the prepared bonding surfaces using a split-mold (3.5 x 5.0 mm). Shear tests (0.5 mm/min) were performed on the specimens (n = 8) after polymerization (control), and after immersion in water at 37 degrees C for 7, 90, and 180 days. All fractured surfaces were examined by scanning electron microscopy (SEM) to calculate the percentage of cohesive fracture (PCF). Shear data were analyzed with 2-way ANOVA and Tukey's test; Kruskall-Wallis test was used to analyze PCF data (alpha= 0.05).
After 90 days water immersion, an increase in the mean SBS was observed for U (11.13 to 16.53 MPa; p < 0.001) and T (9.08 to 13.24 MPa, p= 0.035), whereas resin L showed a decrease (21.74 MPa to 14.96 MPa; p < 0.001). The SBS of resins K (8.44 MPa) and N (7.98 MPa) remained unaffected. The mean PCF was lower than 32.6% for K, N, and T, and higher than 65.6% for U and L.
Long-term water immersion did not adversely affect the bond of materials K, N, T, and U and decreased the values of resin L. Materials L and U failed cohesively, and K, N, and T failed adhesively.
研究水浸泡对1种热聚合丙烯酸树脂(Lucitone 550-L)与4种自聚合重衬树脂(Kooliner-K、New Truliner-N、Tokuso Rebase Fast-T、Ufi Gel Hard-U)之间剪切粘结强度(SBS)的影响。还对用树脂L重衬的试件进行了评估。
加工160个L型义齿基托树脂圆柱体(20×20mm),使用分体模具(3.5×5.0mm)将重衬树脂填充在制备好的粘结面上。聚合后(对照)以及在37℃水中浸泡7、90和180天后,对试件(n = 8)进行剪切试验(0.5mm/min)。通过扫描电子显微镜(SEM)检查所有断裂面,以计算内聚断裂百分比(PCF)。用双向方差分析和Tukey检验分析剪切数据;用Kruskal-Wallis检验分析PCF数据(α = 0.05)。
水浸泡90天后,观察到U树脂(从11.13MPa增至16.53MPa;p < 0.001)和T树脂(从9.08MPa增至13.24MPa,p = 0.035)的平均SBS增加,而树脂L显示出降低(从21.74MPa降至14.96MPa;p < 0.001)。K树脂(8.44MPa)和N树脂(7.98MPa)的SBS保持不变。K、N和T的平均PCF低于32.6%,U和L的平均PCF高于65.6%。
长期水浸泡对材料K、N、T和U的粘结没有不利影响,降低了树脂L的值。材料L和U发生内聚破坏,K、N和T发生粘结破坏。