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水浸对椅旁重衬与义齿基托丙烯酸树脂之间剪切粘结强度的影响。

The effect of water immersion on the shear bond strength between chairside reline and denture base acrylic resins.

作者信息

Azevedo Andrea, Machado Ana Lucia, Giampaolo Eunice Teresinha, Pavarina Ana Claudia, Vergani Carlos Eduardo

机构信息

Department of Dental Materials and Prosthodontics, Araquara Dental School, UNESP - São Paulo State University, Araraquara, São Paulo, Brazil.

出版信息

J Prosthodont. 2007 Jul-Aug;16(4):255-62. doi: 10.1111/j.1532-849X.2007.00188.x. Epub 2007 Apr 23.

Abstract

PURPOSE

The effect of water immersion on the shear bond strength (SBS) between 1 heat-polymerizing acrylic resin (Lucitone 550-L) and 4 autopolymerizing reline resins (Kooliner-K, New Truliner-N, Tokuso Rebase Fast-T, Ufi Gel Hard-U) was investigated. Specimens relined with resin L were also evaluated.

MATERIALS AND METHODS

One hundred sixty cylinders (20 x 20 mm) of L denture base resin were processed, and the reline resins were packed on the prepared bonding surfaces using a split-mold (3.5 x 5.0 mm). Shear tests (0.5 mm/min) were performed on the specimens (n = 8) after polymerization (control), and after immersion in water at 37 degrees C for 7, 90, and 180 days. All fractured surfaces were examined by scanning electron microscopy (SEM) to calculate the percentage of cohesive fracture (PCF). Shear data were analyzed with 2-way ANOVA and Tukey's test; Kruskall-Wallis test was used to analyze PCF data (alpha= 0.05).

RESULTS

After 90 days water immersion, an increase in the mean SBS was observed for U (11.13 to 16.53 MPa; p < 0.001) and T (9.08 to 13.24 MPa, p= 0.035), whereas resin L showed a decrease (21.74 MPa to 14.96 MPa; p < 0.001). The SBS of resins K (8.44 MPa) and N (7.98 MPa) remained unaffected. The mean PCF was lower than 32.6% for K, N, and T, and higher than 65.6% for U and L.

CONCLUSIONS

Long-term water immersion did not adversely affect the bond of materials K, N, T, and U and decreased the values of resin L. Materials L and U failed cohesively, and K, N, and T failed adhesively.

摘要

目的

研究水浸泡对1种热聚合丙烯酸树脂(Lucitone 550-L)与4种自聚合重衬树脂(Kooliner-K、New Truliner-N、Tokuso Rebase Fast-T、Ufi Gel Hard-U)之间剪切粘结强度(SBS)的影响。还对用树脂L重衬的试件进行了评估。

材料与方法

加工160个L型义齿基托树脂圆柱体(20×20mm),使用分体模具(3.5×5.0mm)将重衬树脂填充在制备好的粘结面上。聚合后(对照)以及在37℃水中浸泡7、90和180天后,对试件(n = 8)进行剪切试验(0.5mm/min)。通过扫描电子显微镜(SEM)检查所有断裂面,以计算内聚断裂百分比(PCF)。用双向方差分析和Tukey检验分析剪切数据;用Kruskal-Wallis检验分析PCF数据(α = 0.05)。

结果

水浸泡90天后,观察到U树脂(从11.13MPa增至16.53MPa;p < 0.001)和T树脂(从9.08MPa增至13.24MPa,p = 0.035)的平均SBS增加,而树脂L显示出降低(从21.74MPa降至14.96MPa;p < 0.001)。K树脂(8.44MPa)和N树脂(7.98MPa)的SBS保持不变。K、N和T的平均PCF低于32.6%,U和L的平均PCF高于65.6%。

结论

长期水浸泡对材料K、N、T和U的粘结没有不利影响,降低了树脂L的值。材料L和U发生内聚破坏,K、N和T发生粘结破坏。

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