Garoushi Sufyan, Vallittu Pekka K, Watts David C, Lassila Lippo V J
Department of Prosthetic Dentistry & Biomaterials Science, Institute of Dentistry, University of Turku, Turku, Finland.
Dent Mater. 2008 Feb;24(2):211-5. doi: 10.1016/j.dental.2007.04.001. Epub 2007 May 24.
The aim of this study was to determine the magnitude of short fiber-reinforced composite resin, with a semi-IPN-polymer matrix, on polymerization resin shrinkage-strain, shrinkage stress and marginal microleakage of the restoration.
Experimental composite FC resin was prepared by mixing 22.5 wt.% of short E-glass fibers, 22.5 wt.% of IPN-resin and 55 wt.% of silane treated silica fillers using a high speed mixing machine. As control material, commercial particulate filler composite resin (PFC) was used. Polymerization shrinkage-strain and stress of the specimens (n=5) were measured using the bonded-disc technique and tensilometer, respectively with respect to time. FC composite and PFC were placed incrementally in class II cavities sized 4 mm x 4 mm x 6 mm (n=8/group) using total-etch adhesive system according to manufacturer's instructions. After the class II restorations were completed, the specimens were finished and polished, thermocycled, stained, sectioned, and viewed under a stereo-microscope for leakage at occlusal/enamel and gingival/dentin margins. The data were analyzed using ANOVA.
ANOVA revealed that restorations made from experimental FC composite had a significantly lower shrinkage stress and microleakage than those made from PFC (p<0.05). The data show that gingival margins had higher microleakage than that obtained from occlusal margins of restorations (p<0.05).
The use of short fiber filler with semi-IPN polymer matrix reduced polymerization shrinkage stress and microleakage compared to a conventional restorative composite.
本研究旨在确定具有半互穿聚合物网络(semi-IPN)聚合物基质的短纤维增强复合树脂对修复体聚合树脂收缩应变、收缩应力和边缘微渗漏的影响程度。
通过使用高速混合机将22.5 wt.%的短E-玻璃纤维、22.5 wt.%的IPN树脂和55 wt.%的硅烷处理的二氧化硅填料混合,制备实验性复合FC树脂。作为对照材料,使用市售的颗粒填料复合树脂(PFC)。分别使用粘结圆盘技术和拉伸计,针对时间测量样本(n = 5)的聚合收缩应变和应力。根据制造商的说明,使用全酸蚀粘结系统将FC复合材料和PFC增量放置在尺寸为4 mm×4 mm×6 mm的II类窝洞中(n = 8/组)。完成II类修复后,对样本进行修整和抛光,并进行热循环、染色、切片,然后在立体显微镜下观察咬合/牙釉质和牙龈/牙本质边缘的渗漏情况。使用方差分析(ANOVA)对数据进行分析。
方差分析显示,由实验性FC复合材料制成的修复体的收缩应力和微渗漏明显低于由PFC制成的修复体(p < 0.05)。数据表明,修复体牙龈边缘的微渗漏高于咬合边缘(p < 0.05)。
与传统修复性复合材料相比,使用具有半互穿聚合物网络聚合物基质的短纤维填料可降低聚合收缩应力和微渗漏。