Shiu Peter, De Souza-Zaroni Wanessa Christine, Eduardo Carlos de Paula, Youssef Michel Nicolau
Department of Restorative Dentistry, School of Dentistry, University of São Paulo, São Paulo, Brazil.
Photomed Laser Surg. 2007 Aug;25(4):291-6. doi: 10.1089/pho.2007.2018.
The objective of this study was to evaluate the shear bond strength of resin cement to feldspathic ceramic with various surface treatments.
Application of adhesive techniques is well established in restorative dentistry, yet the influence of surface treatments on the bond strength of resin cement to ceramic materials prior to luting or repair procedures remains unclear.
One hundred samples made of a feldspathic ceramic were divided into 10 groups (n = 10): (1) control (no treatment); (2) 10% hydrofluoric acid (HF); (3) 37% phosphoric acid (H(3)PO(4)); (4) 1.23% acidulated phosphate fluoride acid (APF); (5) diamond bur; (6) air abrasion with Al(2)O(3); (7) Al(2)O(3) + HF; (8) CoJet-Sand; (9) Er:YAG laser, and (10) Al(2)O(3) + Er:YAG laser. Afterwards, silane was applied and a resin cement cylinder was built. After 24 hours at 37 degrees C, the prepared specimens were submitted to a shear bond strength test and stereoscopic evaluation to determine the type of failure after rupture.
Bond strength means were statistically different for the different surface treatments. The highest bond strengths were obtained with HF, CoJet-Sand, and Al(2)O(3). The groups treated with Al(2)O(3) + Er:YAG laser, diamond bur, and Al(2)O(3) + HF had moderate bond strengths. The lowest bond strengths were obtained with H(3)PO(4), APF, Er:YAG laser, and the control group.
The HF, CoJet-Sand, and Al(2)O(3) techniques were the most effective surface treatments. The null surface treatment proposed with the Er:YAG laser showed low bond strength, and seems to be inadequate for clinical use with the parameters tested.
本研究的目的是评估经过各种表面处理的树脂水门汀与长石质陶瓷之间的剪切粘结强度。
粘结技术在口腔修复学中已得到广泛应用,但在粘结或修复操作之前,表面处理对树脂水门汀与陶瓷材料粘结强度的影响仍不明确。
将100个由长石质陶瓷制成的样本分为10组(每组n = 10):(1)对照组(未处理);(2)10%氢氟酸(HF);(3)37%磷酸(H₃PO₄);(4)1.23%酸化磷酸氟(APF);(5)金刚砂车针;(6)用Al₂O₃进行空气喷砂;(7)Al₂O₃ + HF;(8)CoJet-Sand;(9)Er:YAG激光,以及(10)Al₂O₃ + Er:YAG激光。之后,施加硅烷并构建树脂水门汀圆柱体。在37℃下放置24小时后,对制备好的样本进行剪切粘结强度测试和立体评估,以确定断裂后的失效类型。
不同表面处理的粘结强度均值在统计学上存在差异。使用HF、CoJet-Sand和Al₂O₃获得了最高的粘结强度。用Al₂O₃ + Er:YAG激光、金刚砂车针和Al₂O₃ + HF处理的组具有中等粘结强度。使用H₃PO₄、APF、Er:YAG激光处理的组以及对照组获得了最低的粘结强度。
HF、CoJet-Sand和Al₂O₃技术是最有效的表面处理方法。用Er:YAG激光进行的空白表面处理显示出较低的粘结强度,对于所测试的参数,似乎不适合临床使用。