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陶瓷表面处理对陶瓷托槽剪切粘结强度的影响。

Influence of ceramic surface treatment on shear bond strength of ceramic brackets.

作者信息

Ramos Tatiana Fernandes, Lenza Marcos Augusto, Reges Rog Rio Vieira, Freitas Gersinei

机构信息

Department of Orthodontics, Federal University of Goiás, Goiânia and UNIP- Câmpus, Goiânia, Brazil.

出版信息

Indian J Dent Res. 2012 Nov-Dec;23(6):789-94. doi: 10.4103/0970-9290.111261.

Abstract

OBJECTIVE

To compare four different surface treatment methods and determine which produces adequate bond strength between ceramic brackets and facets of porcelain (feldspathic), and evaluate the Adhesive Remnant Index (ARI) scores.

MATERIALS AND METHODS

Ten facets of porcelain specimens with glazed surfaces were used for each group. The specimens were randomly assigned to one of the following treatment conditions of the porcelain surface: (1) no surface treatment (control group), (2) fine diamond bur + orthophosphoric acid gel 37%, (3) hydrofluoric acid (HFL) 10%, and (4) HFL 10% + silane. Ceramic brackets were bonded with the adhesive cement Transbond XT. The shear bond strength values were measured on a universal testing machine at a crosshead speed of 0.5 mm/min.

RESULTS

There was a significant difference (P<0.05) between the control group and all other groups. There was no significant difference (P<0.05) between treated porcelain surface with diamond bur + orthophosphoric acid gel 37% (4.8 MPa) and HFL 10% (6.1 MPa), but the group treated with HFL 10% had clinically acceptable bond strength values. The group treated with HFL 10% + silane (17.5 MPa) resulted in a statistically significant higher tensile bond strength (P<0.05). In group 4, 20% of the porcelain facets displayed damage.

CONCLUSION

Etching of the surface with HFL increased the bond strength values. Silane application was recommended to bond a ceramic bracket to the porcelain surface in order to achieve bond strengths that are clinically acceptable.

摘要

目的

比较四种不同的表面处理方法,确定哪种方法能在陶瓷托槽与瓷(长石质)小平面之间产生足够的粘结强度,并评估粘结剂残留指数(ARI)评分。

材料与方法

每组使用10个带有釉面的瓷标本小平面。将标本随机分配到以下瓷表面处理条件之一:(1)不进行表面处理(对照组),(2)细金刚石车针+37%正磷酸凝胶,(3)10%氢氟酸(HFL),(4)10% HFL+硅烷。使用Transbond XT粘结剂将陶瓷托槽粘结。在万能试验机上以0.5mm/min的十字头速度测量剪切粘结强度值。

结果

对照组与所有其他组之间存在显著差异(P<0.05)。用细金刚石车针+37%正磷酸凝胶处理的瓷表面(4.8MPa)与10% HFL处理的瓷表面(6.1MPa)之间无显著差异(P<0.05),但10% HFL处理组的粘结强度值在临床上是可接受的。10% HFL+硅烷处理组(17.5MPa)的拉伸粘结强度在统计学上显著更高(P<0.05)。在第4组中,20%的瓷小平面出现损伤。

结论

用HFL蚀刻表面可提高粘结强度值。建议使用硅烷将陶瓷托槽粘结到瓷表面,以获得临床上可接受的粘结强度。

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