反相高效液相色谱法测定蓝莓中的多菌灵
Determination of carbendazim in blueberries by reversed-phase high-performance liquid chromatography.
作者信息
Bushway R J, Hurst H L, Kugabalasooriar J, Perkins L B
机构信息
Department of Food Science, University of Maine, Orono 04469.
出版信息
J Chromatogr. 1991 Dec 20;587(2):321-4. doi: 10.1016/0021-9673(91)85176-g.
A fluorescent reversed-phase high-performance liquid chromatographic method was developed for the analysis of carbendazim in blueberries. Recoveries of fortified blueberries at 27 and 810 ng/g were more than adequate with good precision. Forty commercial blueberry samples were analyzed and the amount of carbendazim ranged from none detected (detection limit of 15 ng/g) to 155 ng/g. Confirmation of carbendazim in the blueberry samples was made by enzyme immunoassay and UV photodiode array.
建立了一种荧光反相高效液相色谱法用于分析蓝莓中的多菌灵。在27和810 ng/g添加水平下，强化蓝莓的回收率良好且精度高。对40个市售蓝莓样品进行了分析，多菌灵含量从未检出（检测限为15 ng/g）到155 ng/g不等。通过酶免疫测定法和紫外光电二极管阵列对蓝莓样品中的多菌灵进行了确证。
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