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Synthesis of bisbenzannulated spiroketals-model studies for a modular approach to rubromycins.
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Investigation of a convergent route to purpuromycin: benzofuran formation vs spiroketalization.
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Synthesis of electron deficient 5,6-aryloxy spiroketals.
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Use of a sonogashira-acetylide coupling strategy for the synthesis of the aromatic spiroketal skeleton of gamma-rubromycin.
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Inhibition of telomerase by BIBR 1532 and related analogues.
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The Total Synthesis of Heliquinomycinone This work was supported by the National Institutes of Health (Grant numbers: AI 16943 and HL25848). The authors thank Dr. Makoto Chino of Nippon Kayaku Co., Ltd. for kindly providing a sample of heliquinomycin, and Yashuiro Itagaki of Columbia University for high-resolution mass spectral analyses.
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Studies in the Total Synthesis of Heliquinomycinone: Proof of Concept and Assembly of a Fully Mature Spirocyclization Precursor This work was supported by the National Institutes of Health (Grant numbers: AI 16943 and HL25848). A Postdoctoral Fellowship is gratefully acknowledged by R.X.R. (NIH, Grant Number IF32EY06750-0181). The authors thank Dr. Daniel Chen for important initial experiments, Dr. Brian Bridgewater and Prof. Ged Parkin of Columbia University for X-ray crystal structure analysis of 11 a, and Yashuiro Itagaki for high-resolution mass spectral analyses.
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Mechanism of human telomerase inhibition by BIBR1532, a synthetic, non-nucleosidic drug candidate.
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