1,4 - 二酮衍生物异构体的完整氢谱（¹H NMR）和碳谱（¹³C NMR）归属以及Z/E - 立体构型测定
Complete 1H and 13C NMR assignments and Z/E-stereoconfiguration determination of isomers of 1,4-diketone derivatives.
作者信息
Xu Guohua, Yin Guodong, Guo Wenbo, Wu Anxin, Cui Yanfang
机构信息
Key Laboratory of Pesticide and Chemical Biology, Ministry of Education, Central China Normal University, 152 Luoyu Road, Wuhan 430079, People's Republic of China.
出版信息
Magn Reson Chem. 2008 Jan;46(1):84-7. doi: 10.1002/mrc.2103.
DOI:10.1002/mrc.2103
PMID:18098223
Abstract
Complete 1H and 13C NMR assignments and Z/E-stereoconfiguration determination for a series of new isomers of 1,4-diketone derivatives obtained via self-sorting tandem reaction were accomplished by means of one- and two-dimentional NMR experiments including 1H, 13C, gCOSY, gHSQC, gHMBC, and NOESY.
摘要
通过一维和二维核磁共振实验（包括¹H、¹³C、gCOSY、gHSQC、gHMBC和NOESY），完成了通过自分类串联反应获得的一系列1,4 - 二酮衍生物新异构体的¹H和¹³C核磁共振全归属以及Z/E立体构型测定。
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