Hayakawa T, Horie K
Nihon University School of Dentistry at Matsudo.
Dent Mater J. 1991 Dec;10(2):165-71. doi: 10.4012/dmj.10.165.
Seven types of amide monomers, methacryloyl tyrosine amide (MTYA), p-methacryloxybenzamide (p-MBA), p-methacryloxybutoxybenzamide (p-MBBA), o-methacryloxybutoxybenzamide (o-MBBA), p-methacryloxybutoxy phenylpropionamide (p-MBPPA), 3,5-dimethacryloxybenzamide (3,5-DMBA), and 3,5-di (methacryloxybutoxy)benzamide (3,5-DMBBA), were prepared for use as bonding agents. The monomers were dissolved in HEMA. Bovine enamel was etched with 40% phosphoric acid, and bovine dentin was etched with 10% citric acid before being primed with MTYA.G.H. The tensile bond strengths between bovine enamel or dentin and experimental adhesives were measured after one day immersion in water at 37 degrees C. HEMA was used as a control adhesive. When bonding to etched enamel, the bond strengths of composite resins with o-MBBA and 3,5-DMBA were significantly higher than those with HEMA. The bond strengths of composites with MTYA, p-MBA, p-MBBA, 3,5-DMBBA and p-MBPPA were almost the same as those with HEMA. When bonding to dentin, the bond strengths of composite resin with MTYA and p-MBBA were significantly higher than those with HEMA.
制备了七种酰胺单体,即甲基丙烯酰酪氨酸酰胺(MTYA)、对甲基丙烯酰氧基苯甲酰胺(p-MBA)、对甲基丙烯酰氧基丁氧基苯甲酰胺(p-MBBA)、邻甲基丙烯酰氧基丁氧基苯甲酰胺(o-MBBA)、对甲基丙烯酰氧基丁氧基苯丙酰胺(p-MBPPA)、3,5-二甲基丙烯酰氧基苯甲酰胺(3,5-DMBA)和3,5-二(甲基丙烯酰氧基丁氧基)苯甲酰胺(3,5-DMBBA),用作粘结剂。将这些单体溶解于甲基丙烯酸羟乙酯(HEMA)中。用40%磷酸蚀刻牛牙釉质,用10%柠檬酸蚀刻牛牙本质,然后用MTYA进行预处理。在37℃水中浸泡一天后,测量牛牙釉质或牙本质与实验性粘合剂之间的拉伸粘结强度。使用HEMA作为对照粘合剂。当粘结到蚀刻后的牙釉质上时,含o-MBBA和3,5-DMBA的复合树脂的粘结强度显著高于含HEMA的复合树脂。含MTYA、p-MBA、p-MBBA、3,5-DMBBA和p-MBPPA的复合材料的粘结强度与含HEMA的复合材料几乎相同。当粘结到牙本质上时,含MTYA和p-MBA的复合树脂的粘结强度显著高于含HEMA的复合树脂。