Laboratory for Chemical Engineering, Delft University of Technology, Julianalaan 136, 2628 BL Delft, The Netherlands.
Biotechnol Bioeng. 1982 Feb;24(2):443-59. doi: 10.1002/bit.260240214.
Residence-time-distribution experiments for the fluid in a 30-m(3) pilot plant and a 200-m(3) prototype upflow reactor were performed by means of continuous injection of an LiCl solution as a tracer in the influent of the reactor and measurement of the response of this stimulus on several location in the reactor and in the effluent. In a similar way as described in an article published earlier, models have been developed by use of the measured data of the fluid flow pattern which consisted of region of ideal mixing, plug flow, dead space, and short circuiting. It appeared that the fluid flow patterns in the two reactors were to a large extent analogous. For the pilot plant, three-mixer models appeared to be appropriate while for the prototype reactor two-mixer models have been found. This differences was a result of the difference in the heights of the sludge beds in the reactors: 2-3 m in the pilot plant and only 0.4 m in the prototype reactor, a result of too small an amount of sludge. Another differences was that, due to large amount of mud in the prototype reactor, a region of dead space occurred in the models for the fluid flow pattern in this reactor. The dimension of the prototype reactor have been chosen according to several recommendations obtained from work with the pilot plant (e.g., scale-up should be done by increasing the cross section of the reactor; one influent point should be applied per 5 m(2) bottom surface). The results presented here clearly show the value of these recommendations.
采用连续注入 LiCl 溶液作为示踪剂的方法,对 30m³中试工厂和 200m³上流型反应器中的流体进行停留时间分布实验,并测量该刺激在反应器的几个位置以及出口处的响应。以先前发表的一篇文章中描述的类似方式,使用由理想混合区、塞流、死区和短路等区域组成的流体流动模式的测量数据,开发了模型。结果表明,两个反应器中的流体流动模式在很大程度上是类似的。对于中试工厂,似乎需要使用三混合器模型,而对于原型反应器,则发现了两混合器模型。这种差异是由于两个反应器中污泥床的高度不同所致:中试工厂中为 2-3m,而原型反应器中仅为 0.4m,这是由于污泥量太少所致。另一个差异是,由于原型反应器中存在大量的泥浆,因此在该反应器的流体流动模式模型中出现了死区。原型反应器的尺寸是根据从中试工厂获得的几项建议选择的(例如,应通过增加反应器的横截面来进行放大;每 5m²底部表面应用一个入口点)。这里呈现的结果清楚地表明了这些建议的价值。