Potentiometric and coulometric titration of 2-thiobarbituric acid.
作者信息
Ciesielski W, Kowalska J, Zakrzewski R
机构信息
Department of Instrumental Analysis, University of Łódź, Lindleya 3, Łódź, Poland.
出版信息
Talanta. 1995 May;42(5):733-6. doi: 10.1016/0039-9140(95)01479-u.
PMID:18966286
Abstract
A new method for the determination of 2-thiobarbituric acid, using its reaction with iodine in an alkaline medium is presented. In the volumetric titration with potentiometric end-point detection, the determinability range is 10-400 micromol (1.4-58 mg). In coulometric titration using the biamperometric end-point detection, 0.1-20 micromol (1.4 x 10(-2)-2.9 mg) of 2-thiobarbituric acid was successfully determined.
摘要
相似文献
1
Potentiometric and coulometric titration of 2-thiobarbituric acid.
Talanta. 1995 May;42(5):733-6. doi: 10.1016/0039-9140(95)01479-u.
2
Iodimetric determination of 2-mercaptopyrimidines.2-巯基嘧啶的碘量法测定
Talanta. 1998 Nov;47(3):745-52. doi: 10.1016/s0039-9140(98)00127-1.
3
Potentiometric and coulometric titration of 6-propyl-2-thiouracil.
Analyst. 1997 May;122(5):491-4. doi: 10.1039/a700137a.
4
Coulometric titration of ketotifen in tablets.
Pharmazie. 2005 Mar;60(3):237-8.
5
A new approach to flow-batch titration. A monosegmented flow titrator with coulometric reagent generation and potentiometric or biamperometric detection.
Anal Bioanal Chem. 2006 Nov;386(6):1921-30. doi: 10.1007/s00216-006-0815-5. Epub 2006 Oct 12.
6
Electrooxidation of iodide in the presence of 4-hydroxycoumarin: application to a simple coulometric titration of 4-hydroxycoumarin.4-羟基香豆素存在下碘化物的电氧化：应用于4-羟基香豆素的简单库仑滴定。
Anal Sci. 2003 Jun;19(6):937-9. doi: 10.2116/analsci.19.937.
7
Potentiometric and voltammetric determination of methimazole.甲巯咪唑的电位滴定法和伏安法测定
J Pharm Biomed Anal. 2003 Dec 4;33(5):1143-7. doi: 10.1016/s0731-7085(03)00431-x.
8
Robust flow-batch coulometric/biamperometric titration system: determination of bromine index and bromine number of petrochemicals.稳健的流动-间歇库仑/双安培滴定系统：石油化工产品溴指数和溴值的测定
Anal Chim Acta. 2007 Sep 26;600(1-2):84-9. doi: 10.1016/j.aca.2006.12.039. Epub 2007 Jan 4.
9
Potentiometric study of end-point detection in the coulometric determination of carbon dioxide.
Talanta. 1989 Apr;36(4):519-24. doi: 10.1016/0039-9140(89)80240-1.
10
Determination of sulfide with chloranilic acid by biamperometric and automatic potentiometric end-point detection with a lead chloranilate selective electrode.使用氯冉酸铅选择性电极通过双安培法和自动电位滴定终点检测法测定硫化物。
Talanta. 1992 Aug;39(8):1007-11. doi: 10.1016/0039-9140(92)80287-n.
Zotero 插件