1H、13C和15N核磁共振光谱以及硝基苯并三唑的互变异构现象
1H, 13C and 15N NMR spectroscopy and tautomerism of nitrobenzotriazoles.
作者信息
Larina Lyudmila I, Milata Viktor
机构信息
A. E. Favorsky Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences, 664033, Russian Federation, Irkutsk.
出版信息
Magn Reson Chem. 2009 Feb;47(2):142-8. doi: 10.1002/mrc.2366.
DOI:10.1002/mrc.2366
PMID:19040197
Abstract
Benzotriazole nitro derivatives were prepared by nitration of the corresponding benzotriazoles and by methylation or cyclization of appropriate nitro-1,2-phenylenediamines. Structures and tautomerism of the nitrobenzotriazoles were studied by multinuclear (1)H, (13)C, (15)N, and 2D NMR spectroscopy and quantum chemistry.
摘要
苯并三唑硝基衍生物通过相应苯并三唑的硝化以及合适的硝基 - 1,2 - 苯二胺的甲基化或环化反应制备。利用多核（1）H、（13）C、（15）N 和二维 NMR 光谱以及量子化学研究了硝基苯并三唑的结构和互变异构现象。
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