A natural abundance 33S solid-state NMR study of layered transition metal disulfides at ultrahigh magnetic field.
作者信息
Sutrisno Andre, Terskikh Victor V, Huang Yining
机构信息
Department of Chemistry, The University of Western Ontario, London, Ontario, Canada N6A 5B7.
出版信息
Chem Commun (Camb). 2009 Jan 8(2):186-8. doi: 10.1039/b817017g. Epub 2008 Nov 19.
DOI:10.1039/b817017g
PMID:19099063
Abstract
Using a series of layered transition metal disulfides we demonstrate that the wide-line natural abundance solid-state NMR spectra of 33S in a less symmetric environment can readily be obtained at ultrahigh magnetic field of 21.1 T and that surprisingly these closely related materials display a wide range of 33S quadrupole coupling constant and chemical shift anisotropy values.
摘要
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