Finzel B C, Ohlendorf D H, Weber P C, Salemme F R
E. I. du Pont de Nemours and Company, Central Research and Development Department, Wilmington, DE 19880-0228.
Acta Crystallogr B. 1991 Aug 1;47 ( Pt 4):558-9. doi: 10.1107/s0108768190012939.
Porcine phospholipase A2 (Mr = 13,980), trigonal, P3(1)21, a = b = 69.4, c = 70.4 A, one molecule per asymmetric unit, lambda (Cu K alpha) = 1.54 A. Model incorporating 975 protein atoms and eight solvent molecules refined by restrained least-squares fit to a residual R = 0.21 for 6382 reflections from 5 to 2.4 A resolution.
猪磷脂酶A2(分子量=13,980),呈三角晶系,空间群P3(1)21,a = b = 69.4,c = 70.4埃,每个不对称单位含一个分子,λ(铜Kα射线)= 1.54埃。该模型包含975个蛋白质原子和8个溶剂分子,通过约束最小二乘法拟合进行精修,对于5至2.4埃分辨率下的6382个反射,残余R值为0.21。