皮质类固醇21-葡糖醛酸苷：通过氢核磁共振（¹H NMR）和碳核磁共振（¹³C NMR）进行合成及全面表征
Corticosteroids 21-glucuronides: synthesis and complete characterization by (1)H and (13)C NMR.
作者信息
Ciuffreda Pierangela, Casati Silvana, De Mieri Maria, Ferraboschi Patrizia
机构信息
Dipartimento di Scienze Precliniche LITA Vialba, Università degli Studi di Milano, 20157 Milano, Italy.
出版信息
Steroids. 2009 Oct;74(10-11):870-5. doi: 10.1016/j.steroids.2009.06.003. Epub 2009 Jun 16.
Abstract
Despite the important physiological role of the corticosteroids glucuronides, very poor NMR data for this class of compounds are reported. For this reason we prepared a set of corticosteroids and submitted them to a detailed NMR study. A complete assignment of (1)H and (13)C signals was accomplished arranging mono- and two-dimensional NMR techniques.
摘要
尽管皮质类固醇葡糖醛酸苷具有重要的生理作用，但关于这类化合物的核磁共振（NMR）数据却非常匮乏。因此，我们制备了一组皮质类固醇，并对其进行了详细的核磁共振研究。通过运用一维和二维核磁共振技术，完成了氢（¹H）和碳（¹³C）信号的完全归属。
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