Fischer Jens, Ebinger Andreas, Hägi Tobias, Stawarczyk Bogna, Wenger Andreas, Keller Egbert
Department of Fixed and Removable Prosthodontics and Dental Materials, Center for Dental and Oral Medicine, University of Zurich, Zurich, Switzerland.
Dent Mater. 2009 Nov;25(11):1376-82. doi: 10.1016/j.dental.2009.06.012. Epub 2009 Aug 7.
Aim of the study was to analyze the mold filling capacity and the dimensional accuracy of a spinel-based investment for titanium castings.
Expansion of the investment in dependence of the preheating temperature was measured in a dilatometer. The degree of transformation of MgO and Al2O3 to spinel (MgAl2O4) was evaluated by means of X-ray powder diffraction. Mold filling capacity was assessed by casting a grid and calculating the percentage of completed segments. Dimensional accuracy was analyzed by casting a hollow cylinder and measuring the difference between the inner diameter of the resin pattern and the resulting titanium casting.
Spinel formation starts at 819 degrees C. Diffraction patterns prove the formation of spinel from MgO and Al2O3. The amount of spinel increases with increasing preheating temperature. The final expansion of the investment at the end of the preheating cycle at 450 degrees C shows a linear correlation to the maximum preheating temperature. The degree of mold filling is reciprocal to the preheating temperature. The dimensional accuracy shows a linear correlation to the amount of spinel. Best dimensional accuracy was obtained at about 900 degrees C. After a preheating temperature of 884 degrees C, as recommended by the manufacturer, the cast specimens showed a slightly lower inner diameter as compared to the resin patterns.
The results suggest that with the spinel investment analyzed an excellent accuracy of titanium castings may be obtained.
本研究旨在分析一种用于钛铸件的尖晶石基包埋材料的充型能力和尺寸精度。
在膨胀仪中测量包埋材料随预热温度变化的膨胀情况。通过X射线粉末衍射评估MgO和Al2O3向尖晶石(MgAl2O4)的转变程度。通过铸造一个网格并计算完成部分的百分比来评估充型能力。通过铸造一个空心圆柱体并测量树脂模型的内径与最终钛铸件内径之间的差异来分析尺寸精度。
尖晶石的形成始于819℃。衍射图谱证明了MgO和Al2O3形成了尖晶石。尖晶石的量随预热温度的升高而增加。在450℃预热周期结束时,包埋材料的最终膨胀与最高预热温度呈线性相关。充型程度与预热温度呈反比。尺寸精度与尖晶石的量呈线性相关。在约900℃时获得最佳尺寸精度。按照制造商推荐的884℃预热温度后,铸造的试样与树脂模型相比,内径略小。
结果表明,对于所分析的尖晶石包埋材料,可获得优异的钛铸件精度。