Kazimirov A, Kohn V G, Snigirev A, Snigireva I
Cornell High Energy Synchrotron Source, Cornell University, Ithaca, NY 14853, USA.
J Synchrotron Radiat. 2009 Sep;16(Pt 5):666-71. doi: 10.1107/S0909049509029860. Epub 2009 Aug 14.
The spatial structure of a beam focused by a planar refractive lens and Bragg diffracted from perfect silicon crystals was experimentally studied at the focal plane using a knife-edge scan and a high-resolution CCD camera. The use of refractive lenses allowed for a detailed comparison with theory. It was shown that diffraction leads to broadening of the focused beam owing to the extinction effect and, for a sufficiently thin crystal, to the appearance of a second peak owing to reflection from the back surface. It was found that the spatial structure of the diffracted beam depends on whether the crystal diffracts strongly (dynamically) or weakly (kinematically). The results help to understand the physical origin of the diffracted intensity recorded in a typical microbeam diffraction experiment.
利用刀口扫描和高分辨率电荷耦合器件(CCD)相机,在焦平面上对由平面折射透镜聚焦并从完美硅晶体进行布拉格衍射的光束的空间结构进行了实验研究。折射透镜的使用使得能够与理论进行详细比较。结果表明,由于消光效应,衍射会导致聚焦光束变宽,并且对于足够薄的晶体,由于后表面反射会出现第二个峰值。研究发现,衍射光束的空间结构取决于晶体是强(动态)衍射还是弱(运动学)衍射。这些结果有助于理解在典型的微束衍射实验中记录的衍射强度的物理起源。