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基于短棒、人字形切口试验的双层牙科陶瓷的界面韧性。

Interfacial toughness of bilayer dental ceramics based on a short-bar, chevron-notch test.

机构信息

Department of Dental Biomaterials, College of Dentistry, University of Florida, Gainesville, FL, USA.

出版信息

Dent Mater. 2010 Feb;26(2):111-7. doi: 10.1016/j.dental.2009.09.003. Epub 2009 Oct 8.

Abstract

OBJECTIVE

The objective of this study was to test the null hypothesis that the interfacial toughness of each of two types of bonded core-veneer bilayer ceramics is not significantly different from the apparent fracture toughness of the control monolithic glass veneer.

METHODS

T-shaped short-bars of a lithia-disilicate glass-ceramic core (LC) and yttria-stabilized polycrystalline zirconia core ceramic (ZC) were prepared according to the manufacturer's recommendations. V-shaped notches were prepared by using 25-mum-thick palladium foil, leaving the chevron-notch area exposed, and the bars were veneered with a thermally compatible glass veneer (LC/GV and ZC/GV). Additionally, we also bonded the glass veneer to itself as a control group (GV/GV). Specimens were kept in distilled water for 30 days before testing in tension. Eight glass veneer bars were prepared for the analysis of fracture toughness test using the indentation-strength technique.

RESULTS

The mean interfacial toughness of the LC/GV group was 0.69 MPam(1/2) (0.11), and did not significantly differ from that of the GV/GV control group, 0.74 MPam(1/2) (0.17) (p>0.05). However, the difference between the mean interfacial toughness of the ZC/GV group, 0.13 MPam(1/2) (0.07), and the LC/GV and the GV/GV groups was statistically significant (p<0.05).

SIGNIFICANCE

For bilayer all-ceramic restorations with high-strength core materials, the veneering ceramics are the weakest link in the design of the structure. Since all-ceramic restorations often fail from chipping of veneer layers or crack initiation at the interface, the protective effects of thermal mismatch stresses oral prosthesis design should be investigated.

摘要

目的

本研究的目的是验证以下假设,即两种粘结的核-面层双层陶瓷的界面韧性与对照单片玻璃层的表观断裂韧性无显著差异。

方法

根据制造商的建议,制备锂硅玻璃陶瓷核(LC)和氧化钇稳定的多晶氧化锆核陶瓷(ZC)的 T 型短棒。使用 25μm 厚的钯箔制备 V 型缺口,留下人字形缺口区域暴露,棒被热相容的玻璃层(LC/GV 和 ZC/GV)包层。此外,我们还将玻璃层自身粘结作为对照组(GV/GV)。在张力测试前,将试件在蒸馏水中保存 30 天。使用压痕强度技术对 8 个玻璃层进行断裂韧性测试的分析。

结果

LC/GV 组的界面韧性平均值为 0.69 MPam(1/2)(0.11),与 GV/GV 对照组(0.74 MPam(1/2)(0.17))无显著差异(p>0.05)。然而,ZC/GV 组的界面韧性平均值(0.13 MPam(1/2)(0.07))与 LC/GV 组和 GV/GV 组之间的差异具有统计学意义(p<0.05)。

意义

对于高强度核材料的双层全瓷修复体,包层陶瓷是结构设计中的最薄弱环节。由于全瓷修复体通常从面层层剥落或在界面处起始裂纹而失效,因此应该研究热失配应力或口腔修复体设计的保护作用。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/95dc/2815119/c2f260f93f38/nihms-146443-f0001.jpg

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