超声辐射下，由苯乙酮和芳香醛直接一锅法合成 2,3-环氧-1,3-二芳基-1-丙酮。
An efficient one-pot synthesis of 2,3-epoxyl-1,3-diaryl-1-propanone directly from acetophenones and aromatic aldehydes under ultrasound irradiation.
机构信息
College of Chemistry and Environmental Science, Hebei University, Baoding, PR China.
出版信息
Ultrason Sonochem. 2010 Feb;17(2):363-6. doi: 10.1016/j.ultsonch.2009.09.007. Epub 2009 Sep 26.
Abstract
A convenient and efficient one-pot synthesis of 2,3-epoxyl-1,3-diaryl-1-propanone directly from acetophenones and aromatic aldehydes under ultrasound irradiation at room temperature has been described. In comparison to two-step methods, the present procedure has the advantages of mild conditions, shorter reaction time, without isolation of any intermediate, saves energy and no requirement of toxic solvent.
摘要
在超声辐射下，室温下直接从苯乙酮和芳香醛方便、高效地一锅合成了 2,3-环氧-1,3-二芳基-1-丙酮。与两步法相比，本方法具有条件温和、反应时间短、无需分离任何中间产物、节能、无需使用有毒溶剂等优点。
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