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[Simultaneous determination of PAHs in food by low-temperature constant-energy synchronous fluorescence spectrometry].

作者信息

Zhang Wei, Zhou Na, Li Na, Xie Yong-Sheng, Luo He-Dong, Li Yao-Qun

机构信息

Department of Chemistry, The Key Laboratory of Analytical Sciences of the Ministry of Education, College of Chemistry and Chemical Engineering, Xiamen University, Xiamen 361005, China.

出版信息

Guang Pu Xue Yu Guang Pu Fen Xi. 2009 Oct;29(10):2806-9.

Abstract

The authors developed a rapid analytical method that could determine the PAHs in food samples simultaneously by the coupled approach of Shpol' skii spectroscopy and constant-energy synchronous fluorescence scanning technique. Low-fat food samples, which were just extracted with octane and high-fat food samples pre-processed with saponification and extracting, could be analyzed immediately. The recoveries ranged from 80.2% to 98.9% and the correlation coefficients of the linearity were higher than 0.993 8. This method was selective, simple, rapid and inexpensive.

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