用葡萄糖氧化酶法测定6-氨基青霉烷酸和7-氨基-3-甲基-Δ3-头孢烯-4-羧酸。
GLC determination of 6-aminopenicillanic acid and 7-amino-3-methyl-delta3-cephem-4-carboxylic acid.
作者信息
Silingardi S, Di Bitetto M, Mangia A
出版信息
J Pharm Sci. 1977 Dec;66(12):1769-71. doi: 10.1002/jps.2600661231.
PMID:200731
Abstract
A quantitative GLC determination of 6-aminopenicillanic acid and 7-amino-3-methyl-delta3-cephem-4-carboxylic acid is presented. The results obtained are in good agreement with those of known chemical procedures. The method is free from interference by related substances.
摘要
本文介绍了一种用气相色谱法定量测定6-氨基青霉烷酸和7-氨基-3-甲基-Δ3-头孢烯-4-羧酸的方法。所得结果与已知化学方法的结果吻合良好。该方法不受相关物质的干扰。
相似文献
1
GLC determination of 6-aminopenicillanic acid and 7-amino-3-methyl-delta3-cephem-4-carboxylic acid.用葡萄糖氧化酶法测定6-氨基青霉烷酸和7-氨基-3-甲基-Δ3-头孢烯-4-羧酸。
J Pharm Sci. 1977 Dec;66(12):1769-71. doi: 10.1002/jps.2600661231.
2
Preparation, identification, and quantitative NMR determination of silyl derivatives of 6-aminopenicillanic acid, 7-amino-3-methyl-delta3-cephem-4-carboxylic acid, and 7-amino-3-acetoxymethyl-delta3-cephem-4-carboxylic acid.6-氨基青霉烷酸、7-氨基-3-甲基-Δ3-头孢烯-4-羧酸和7-氨基-3-乙酰氧甲基-Δ3-头孢烯-4-羧酸的硅烷基衍生物的制备、鉴定及定量核磁共振测定
J Pharm Sci. 1977 Dec;66(12):1767-9. doi: 10.1002/jps.2600661230.
3
Determination of penicillic acid and patulin by gas-liquid chromatography with an electron-capture detector.
J Chromatogr. 1975 Feb 19;105(1):99-106. doi: 10.1016/s0021-9673(01)81093-1.
4
5
[Determination of ampicillin, cephalexin and related compounds by formol titration. 7. Condensated acetidinones].用甲醛滴定法测定氨苄西林、头孢氨苄及相关化合物。7. 缩合乙酰啶酮类
Arch Pharm (Weinheim). 1972 Jul;305(7):548-53. doi: 10.1002/ardp.19723050712.
6
High-performance liquid chromatographic determination of 6-aminopenicillanic acid by postcolumn alkaline degradation.
Anal Biochem. 1986 Oct;158(1):146-50. doi: 10.1016/0003-2697(86)90602-0.
7
Spectrophotometric determination of 6-aminopenicillanic and 7-aminocephalosporanic acids as the Schiff bases with para-dimethylaminobenzaldehyde in the presence of sodium dodecyl sulfate micelles.
Anal Biochem. 1995 Aug 10;229(2):249-55. doi: 10.1006/abio.1995.1409.
8
A new colorimetric method for the determination of 6-aminopenicillanic acid.一种测定6-氨基青霉烷酸的新比色法。
Anal Biochem. 1978 May;86(1):118-26. doi: 10.1016/0003-2697(78)90324-x.
9
Preparation of trimethylsilyl derivatives of ribonucleosides for gas chromatography.
J Chromatogr. 1985 Nov 27;348(1):280-5. doi: 10.1016/s0021-9673(01)92462-8.
10
[Determination of a dimethylaniline mixture in the intermediate products for the production of semisynthetic penicillins].
Antibiotiki. 1979 May;24(5):328-31.
Zotero 插件