College of Chemistry, Xiangtan University, Key Laboratory of Environmentally Friendly Chemistry and Applications of Ministry of Education, Xiangtan 411105, Hunan, China.
Carbohydr Res. 2010 May 27;345(8):994-8. doi: 10.1016/j.carres.2010.03.019. Epub 2010 Mar 19.
Novel chitosan/ZnO nanoparticle (CS/nano-ZnO) composite membranes were prepared via the method of sol-cast transformation and studied by UV-vis absorption spectroscopy (UV-vis), Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), scanning electron microscopy (SEM), and energy dispersive X-ray fluorescence spectrometry (EDX). The characterization revealed that ZnO nanoparticles dispersed homogeneously within the chitosan matrix. The mechanical and antibacterial properties of the product were investigated. The results showed that the ZnO content had an effect on the mechanical properties of CS/nano-ZnO composite membranes, and that the antibacterial activities of CS membranes for Bacillus subtilis, Escherichia coli, and Staphylococcus aureus were enhanced by the incorporation of ZnO. Further, CS/nano-ZnO composite membranes with 6-10 wt% ZnO exhibited high antibacterial activities.
新型壳聚糖/氧化锌纳米粒子(CS/nano-ZnO)复合膜通过溶胶-凝胶转化法制备,并通过紫外可见吸收光谱(UV-vis)、傅里叶变换红外光谱(FTIR)、X 射线衍射(XRD)、扫描电子显微镜(SEM)和能谱(EDX)进行了研究。表征结果表明,氧化锌纳米粒子均匀分散在壳聚糖基体中。研究了该产物的机械性能和抗菌性能。结果表明,氧化锌含量对 CS/nano-ZnO 复合膜的机械性能有影响,并且氧化锌的加入提高了 CS 膜对枯草芽孢杆菌、大肠杆菌和金黄色葡萄球菌的抗菌活性。此外,含有 6-10wt%氧化锌的 CS/nano-ZnO 复合膜具有较高的抗菌活性。