Chemical Sciences Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831, USA.
Chem Commun (Camb). 2010 Jul 7;46(25):4487-9. doi: 10.1039/c0cc00799d. Epub 2010 May 19.
Stable high-concentration suspensions (up to 0.95 mg mL(-1)) of non-oxidized few layer graphene (FLG), five or less sheets, with micrometre-long edges were obtained via direct exfoliation of natural graphite flakes in ionic liquids, such as 1-butyl-3-methyl-imidazolium bis(trifluoro-methane-sulfonyl)imide ([Bmim]-[Tf(2)N]), by tip ultrasonication.
通过在离子液体(如 1-丁基-3-甲基-咪唑双(三氟甲烷磺酰)亚胺([Bmim]-[Tf(2)N]))中,通过尖端超声处理,直接剥离天然石墨片,得到了稳定的高浓度悬浮液(高达 0.95mg mL(-1))的未氧化的少层石墨烯(FLG),其边缘长达数微米,有五张或更少的薄片。