Li Hai-Long, Zhu Di, Liu Ran-Ran, Chen Tao, Tian Wen-Yu, Sun Mao, Li Chun, Zhao Yu-Liang, Liu Chun-Li
Beijing National Laboratory for Molecular Science, College of Chemistry and Molecular Engineering, Peking University, Beijing 100871, China.
Guang Pu Xue Yu Guang Pu Fen Xi. 2010 Mar;30(3):767-9.
Anatase-type TiO2 fine powders were synthesized under hydrothermal condition. The precursor was obtained via precipitation route using Ti(SO4)2. The characterization of the as-prepared sample was confirmed by TEM, XRD, UV-Vis and low temperature N2 adsorption measurements (BET). The photocatalytic activity was also investigated by the degradation of methyl orange solutions. The particles of the as-synthesized sample with narrow size distribution had an average diameter of about 24 nm. The specific BET surface area of the as-synthesized sample was about 56 m2 x g(-1), which is similar to the commercial TiO2 (P25). The prepared materials showed the similar photocatalytic activity when compared with the performance of commercial TiO2 (P25).
在水热条件下合成了锐钛矿型二氧化钛细粉。前驱体通过使用硫酸钛(Ti(SO4)2)的沉淀法获得。通过透射电子显微镜(TEM)、X射线衍射(XRD)、紫外可见光谱(UV-Vis)和低温氮气吸附测量(BET)对所制备的样品进行了表征。还通过甲基橙溶液的降解研究了光催化活性。所合成样品的颗粒尺寸分布窄,平均直径约为24 nm。所合成样品的比表面积约为56 m2·g-1,与商业二氧化钛(P25)相似。与商业二氧化钛(P25)的性能相比,所制备的材料表现出相似的光催化活性。