Department of Chemistry, Faculty of Sciences, Tarbiat Modares University, P.O. Box 14155-4838, Tehran, Islamic Republic of Iran.
Ultrason Sonochem. 2011 Jan;18(1):375-81. doi: 10.1016/j.ultsonch.2010.07.001. Epub 2010 Jul 6.
In(OH)(3) and In(2)O(3) nano-structures have been synthesized from the reaction of In(CH(3)COO)(3) and sodium hydroxide by a sonochemical method. The effects of reaction conditions, such as the concentration of the In(3+) ion, aging time and power of the ultrasonic device have been investigated. The In(2)O(3) and In(OH)(3) nano-structures were characterized by scanning electron microscopy (SEM), X-ray powder diffraction (XRD), Thermal Gravimetric Analysis (TGA), Differential Thermal Analysis (DTA) and Energy-dispersive X-ray analysis (EDAX) technique.
采用超声化学法，由醋酸铟和氢氧化钠反应合成了 In(OH)(3)和 In(2)O(3)纳米结构。考察了反应条件如[In(3+)]离子浓度、陈化时间和超声功率对反应的影响。用扫描电子显微镜(SEM)、X 射线粉末衍射(XRD)、热重分析(TGA)、差热分析(DTA)和能谱分析(EDAX)技术对 In(2)O(3)和 In(OH)(3)纳米结构进行了表征。
