Varadarajan R, Rimnac C M
Musculoskeletal Mechanics and Materials Laboratories, Department of Mechanical and Aerospace Engineering, Case Western Reserve University, Cleveland, OH 44106, USA.
Polym Test. 2008 Aug 1;27(5):616-620. doi: 10.1016/j.polymertesting.2008.03.007.
Fracture of ultra high molecular weight polyethylene (UHMWPE) total joint replacement components is a clinical concern. Thus, it is important to characterize the fracture resistance of UHMWPE. To determine J-initiation fracture toughness (J(Q)) for metals and metallic alloys, ASTM E1820 recommends a procedure based on an empirical crack blunting line. This approach has been found to overestimate the initiation toughness of tough polymers like UHMWPE. Therefore, in this study, a novel experimental approach based on crack tip opening displacement (CTOD) was utilized to evaluate J(Q) of UHMWPE materials. J-initiation fracture toughness was experimentally measured in ambient air and a physiologically-relevant 37°C PBS environment for three different formulations of UHMWPE and compared to the blunting line approach. The CTOD method was found to provide J(Q) values comparable to the blunting line approach for the UHMWPE materials and environments examined in this study. The CTOD method used in this study is based on experimental observation and, thus, does not rely on an empirical relationship or fracture surface measurements. Therefore, determining J(Q) using the experimentally based CTOD method proposed in this study may be a more reliable approach for UHMWPE and other tough polymers than the blunting line approach.
超高分子量聚乙烯(UHMWPE)全关节置换部件的断裂是一个临床关注的问题。因此,表征UHMWPE的抗断裂性能很重要。为了测定金属和金属合金的J起始断裂韧性(J(Q)),ASTM E1820推荐了一种基于经验裂纹钝化线的方法。已发现这种方法高估了像UHMWPE这样的韧性聚合物的起始韧性。因此,在本研究中,采用了一种基于裂纹尖端开口位移(CTOD)的新型实验方法来评估UHMWPE材料的J(Q)。在环境空气和生理相关的37°C磷酸盐缓冲盐水(PBS)环境中,对三种不同配方的UHMWPE进行了J起始断裂韧性的实验测量,并与钝化线方法进行了比较。结果发现,对于本研究中所研究的UHMWPE材料和环境,CTOD方法所提供的J(Q)值与钝化线方法相当。本研究中使用的CTOD方法基于实验观察,因此不依赖于经验关系或断口测量。因此,与钝化线方法相比,使用本研究中基于实验的CTOD方法来测定J(Q)对于UHMWPE和其他韧性聚合物可能是一种更可靠的方法。