Centro de Investigación en Alimentación y Desarrollo, A.C., Cuauhtémoc, Chih., Mexico.
J Food Sci. 2010 Aug 1;75(6):E347-52. doi: 10.1111/j.1750-3841.2010.01661.x.
Mucilage of Opuntia ficus-indica (OFI) was extracted and characterized by its composition and molecular weight distribution. Mucilage film-forming dispersions were prepared under different pHs (3, 4, 5.6, 7, and 8) and calcium concentration (0% and 30% of CaCl(2), with respect to mucilage's weight), and their particle size determined. Mucilage films with and without calcium (MFCa and MF, respectively) were prepared. The effect of calcium and pH on mucilage films was evaluated determining thickness, color, water vapor permeability (WVP), tensile strength (TS), and percentage of elongation (%E). The average molecular weight of the different fractions of mucilage was: 3.4 x 10(6) (0.73%), 1 x 10(5) (1.46%), 1.1 x 10(3) (45.79%), and 2.4 x 10(2) Da (52.03%). Aqueous mucilage dispersions with no calcium presented particles with an average size d(0.5) of 15.4 microm, greater than the dispersions with calcium, 13.2 microm. MFCa films showed more thickness (0.13 mm) than the MF films (0.10 mm). The addition of calcium increased the WVP of the films from 109.94 to 130.45 gmm/m(2)dkPa. Calcium and pH affected the mechanical properties of the films; the largest TS was observed on MF films, whereas the highest %E was observed on MFCa films. The highest differences among MF and MFCa films were observed at pHs 5.6 and 7 for TS and at pHs 4 and 8 for %E. No effect of pH and calcium was observed on luminosity and hue angle. Chroma values were higher for MF when compared with MFCa, and increased as pH of the films increased. Practical Application: In this study mucilage from nopal was extracted and characterized by its ability to form edible films under different pHs, and with or without the addition of calcium. Opuntia ficus-indica mucilage had the ability to form edible films. In general, it can be considered that mucilage films without modification of pH and without the addition of calcium have the best water vapor barrier properties and tensile strength. Mucilage from nopal could represent a good option for the development of edible films in countries where nopal is highly produced at low cost, constituting a processing alternative for nopal.
仙人掌果(OFI)的黏胶通过其组成和分子量分布进行提取和表征。在不同的 pH 值(3、4、5.6、7 和 8)和不同的钙离子浓度(0%和 30%的 CaCl2,相对于黏胶的重量)下制备黏胶成膜分散体,并确定其粒径。制备了含有和不含有钙的黏胶膜(MFCa 和 MF,分别)。通过测定厚度、颜色、水蒸气透过率(WVP)、拉伸强度(TS)和伸长率(%E)来评估钙和 pH 对黏胶膜的影响。不同黏胶分数的平均分子量为:3.4 x 10(6)(0.73%)、1 x 10(5)(1.46%)、1.1 x 10(3)(45.79%)和 2.4 x 10(2)Da(52.03%)。没有钙的水性黏胶分散体的颗粒平均粒径 d(0.5)为 15.4 微米,大于含钙分散体的 13.2 微米。MFCa 膜的厚度(0.13 毫米)大于 MF 膜(0.10 毫米)。添加钙会使膜的 WVP 从 109.94 增加到 130.45 gmm/m(2)dkPa。钙和 pH 会影响膜的机械性能;MF 膜的最大 TS,而 MFCa 膜的最大伸长率。在 pH 5.6 和 7 时,MF 和 MFCa 膜之间的最大差异在 TS 方面,而在 pH 4 和 8 时在 %E 方面。pH 和钙对亮度和色调角没有影响。与 MFCa 相比,MF 的色值更高,并且随着膜 pH 值的增加而增加。实际应用:在这项研究中,从龙舌兰中提取了黏胶,并通过其在不同 pH 值下形成可食用膜的能力以及是否添加钙来对其进行了表征。仙人掌果黏胶具有形成可食用膜的能力。一般来说,可以认为 pH 值未改性且未添加钙的黏胶膜具有最佳的水蒸气阻隔性能和拉伸强度。龙舌兰黏胶可能是在龙舌兰产量高、成本低的国家开发可食用膜的一个很好的选择,为龙舌兰的加工提供了一个选择。