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影响含纳米填料树脂复合材料修复体边缘间隙适应性的因素。

Factors influencing marginal cavity adaptation of nanofiller containing resin composite restorations.

机构信息

Advanced Biomaterials, Department of Restorative Sciences, Division of Oral Health Sciences, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University, Yushima 1-5-45, Bunkyo-ku, Tokyo 113-8549, Japan.

出版信息

Dent Mater. 2010 Dec;26(12):1166-75. doi: 10.1016/j.dental.2010.08.189. Epub 2010 Sep 29.

Abstract

OBJECTIVES

The aim of this study was to investigate the effects of polymerization contraction, shrinkage stress and Young's modulus of nanofiller containing resin composites on early marginal adaptation of restorations in cavities.

METHODS

Six nanofiller containing and two reference resin composites were studied. Marginal gap widths of restorations in cylindrical 4.2mm wide and 1.5mm deep dentin cavities, non-bonded or bonded with a self-etch adhesive, and in Teflon cavities of same dimensions were determined 15 min after irradiation (n=8). Polymerization shrinkage strains were measured using the bonded-disk (n=8) and a strain gage method (n=8). For determination of contraction stress the composites (n=10) were bonded to and cured in Araldit molds using a photoelastic method. Flexural moduli of the restoratives were studied according to ISO specification 4049 (n=5). Statistical analysis was performed with one- and two-way ANOVA, Kruskal-Wallis ANOVA test and post hoc tests (p<0.05).

RESULTS

Only two nanofiller composites (Kalore, GC, Japan) and Venus Diamond (Heraeus Kulzer, Germany) showed consistently gap-free margins in bonded dentin cavities. The mean gap widths in non-bonded and in Teflon cavities were 6.1-12.8 and 14.1-25.5 μm, and linearly correlated (r(2)<0.85). Significant linear relationships were observed between strain, stress and marginal gap widths in non-bonded and Teflon cavities (p<0.01). Flexural moduli (15 min) were between 1.66 and 8.63 GPa.

SIGNIFICANCE

Marginal cavity adaptation of restorations in bonded dentin cavities reflects complex interactions between adhesive bonding on the one hand, and polymerization contraction strain, stress and elastic modulus, on the other.

摘要

目的

本研究旨在探讨聚合收缩、收缩应力和含纳米填料的树脂复合材料的杨氏模量对窝洞修复体早期边缘适应性的影响。

方法

研究了 6 种含纳米填料和 2 种参比树脂复合材料。15 分钟后,在圆柱形 4.2mm 宽、1.5mm 深的牙本质窝洞(未粘结或用自酸蚀粘结剂粘结)以及相同尺寸的聚四氟乙烯窝洞中,测量修复体的边缘间隙宽度(n=8)。使用粘结盘(n=8)和应变计法(n=8)测量聚合收缩应变。采用光弹性法,将复合材料(n=10)粘结并固化在 Araldit 模具中,以测定收缩应力。根据 ISO 4049 规范(n=5)研究修复体的挠曲模量。采用单因素和双因素方差分析、Kruskal-Wallis ANOVA 检验和事后检验(p<0.05)进行统计分析。

结果

只有 2 种含纳米填料复合材料(Kalore,GC,日本和 Venus Diamond,Heraeus Kulzer,德国)在粘结牙本质窝洞中表现出连续无间隙的边缘。未粘结和聚四氟乙烯窝洞的平均间隙宽度分别为 6.1-12.8μm 和 14.1-25.5μm,呈线性相关(r²<0.85)。在未粘结和聚四氟乙烯窝洞中,应变、应力和边缘间隙宽度之间存在显著的线性关系(p<0.01)。15 分钟时的挠曲模量在 1.66-8.63GPa 之间。

意义

粘结牙本质窝洞修复体的边缘适应性反映了粘结剂粘结与聚合收缩应变、应力和弹性模量之间的复杂相互作用。

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