Irie Masao, Okada Masahiro, Maruo Yukinori, Nishigawa Goro, Matsumoto Takuya
Department of Biomaterials, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Science, 2-5-1 Shikata-cho, Okayama 700-8525, Japan.
Department of Prosthodontics, Division of Dentistry, Okayama University, 2-5-1 Shikata-cho, Okayama 700-8525, Japan.
Polymers (Basel). 2023 Feb 23;15(5):1128. doi: 10.3390/polym15051128.
This study investigates the effect of the curing mode (dual-cure vs. self-cure) of resin cements (four self-adhesive and seven conventional cements) on their flexural strength and flexural modulus of elasticity, alongside their shear bond strength to lithium disilicate ceramics (LDS). The study aims to determine the relationship between the bond strength and LDS, and the flexural strength and flexural modulus of elasticity of resin cements. Twelve conventional or adhesive and self-adhesive resin cements were tested. The manufacturer's recommended pretreating agents were used where indicated. The shear bond strengths to LDS and the flexural strength and flexural modulus of elasticity of the cement were measured immediately after setting, after one day of storage in distilled water at 37 °C, and after 20,000 thermocycles (TC 20k). The relationship between the bond strength to LDS, flexural strength, and flexural modulus of elasticity of resin cements was investigated using a multiple linear regression analysis. For all resin cements, the shear bond strength, flexural strength, and flexural modulus of elasticity were lowest immediately after setting. A clear and significant difference between dual-curing and self-curing modes was observed in all resin cements immediately after setting, except for ResiCem EX. Regardless of the difference of the core-mode condition of all resin cements, flexural strengths were correlated with the LDS surface upon shear bond strengths ( = 0.24, = 69, < 0.001) and the flexural modulus of elasticity was correlated with them ( = 0.14, = 69, < 0.001). Multiple linear regression analyses revealed that the shear bond strength was 17.877 + 0.166, the flexural strength was 0.643, and the flexural modulus was ( = 0.51, = 69, < 0.001). The flexural strength or flexural modulus of elasticity may be used to predict the bond strength of resin cements to LDS.
本研究调查了树脂水门汀(四种自粘接和七种传统水门汀)的固化方式(双固化与自固化)对其弯曲强度、弯曲弹性模量以及与二硅酸锂陶瓷(LDS)的剪切粘结强度的影响。该研究旨在确定粘结强度与LDS之间的关系,以及树脂水门汀的弯曲强度和弯曲弹性模量之间的关系。测试了十二种传统或粘结性及自粘结性树脂水门汀。在有指示的情况下使用了制造商推荐的预处理剂。在固化后、在37℃蒸馏水中储存一天后以及20000次热循环(TC 20k)后,测量了与LDS的剪切粘结强度以及水门汀的弯曲强度和弯曲弹性模量。使用多元线性回归分析研究了树脂水门汀与LDS的粘结强度、弯曲强度和弯曲弹性模量之间的关系。对于所有树脂水门汀,固化后立即测得的剪切粘结强度、弯曲强度和弯曲弹性模量最低。除ResiCem EX外,在所有树脂水门汀固化后立即观察到双固化和自固化模式之间存在明显且显著的差异。无论所有树脂水门汀的核心模式条件如何不同,弯曲强度与剪切粘结强度时的LDS表面相关( = 0.24, = 69, < 0.001),弯曲弹性模量也与之相关( = 0.14, = 69, < 0.001)。多元线性回归分析显示,剪切粘结强度为17.877 + 0.166,弯曲强度为0.643,弯曲模量为( = 0.51, = 69, < 0.001)。弯曲强度或弯曲弹性模量可用于预测树脂水门汀与LDS的粘结强度。