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调节剂对自粘接树脂水门汀与牙本质微拉伸粘接强度的影响。

Effect of conditioner on microtensile bond strength of self-adhesive resin cements to dentin.

作者信息

Tonial Daniela, Ghiggi Paula Cristine, Lise André Amorim, Burnett Luiz Henrique, Oshima Hugo Mitsuo Silva, Spohr Ana Maria

机构信息

Pontifical Catholic University of Rio Grande do Sul (PUCRS), Av. Ipiranga 6681, Porto Alegre, Rio Grande do Sul, Brazil.

出版信息

Stomatologija. 2010;12(3):73-9.

Abstract

OBJECTIVE

Evaluate, in vitro, the microtensile bond strength (µTBS) of RelyX ARC conventional resin cement and RelyX Unicem and Maxcem self-adhesive resin cements to dentin, and the influence of polyacrylic acid pretreatment on the µTBS.

MATERIAL AND METHODS

Flat dentin surfaces were obtained in 15 third molars which were randomly divided into 5 groups: Group 1 - RelyX ARC (control); Group 2 - RelyX Unicem; Group 3 - Maxcem Elite; Group 4 - 22.5% polyacrylic acid and RelyX Unicem; Group 5 - 22.5% polyacrylic acid and Maxcem Elite. A block of composite resin was built over the resin cements. The samples were sectioned to obtain beams, and 20 specimens for each group were submitted to µTBS on a universal testing machine. Failure modes were analyzed by scanning electron microscopy.

RESULTS

According to ANOVA and Tukey test, the highest µTBS mean (MPa) was obtained with RelyX ARC (21.38), which did not differ statistically from Maxcem Elite with polyacrylic acid pretreatment (19.22) and RelyX Unicem with polyacrylic acid pretreatment (17.75) (p>0.05). The latter two groups did not differ statistically from RelyX Unicem (16.98) (p>0.05). The lowest mean was obtained for Maxcem Elite (6.43), which differed statistically from the other groups (p<0.05). All failures were adhesive for Maxcem Elite without polyacrylic acid pretreatment, and mixed failures were predominant in the other groups.

CONCLUSIONS

RelyX ARC achieved higher µTBS to dentin in comparison to the self-adhesive resin cements. Polyacrylic acid pretreatment was effective in improving the µTBS of Maxcem Elite, but did not influence the µTBS for RelyX Unicem.

摘要

目的

在体外评估RelyX ARC传统树脂水门汀、RelyX Unicem和Maxcem自粘树脂水门汀与牙本质之间的微拉伸粘结强度(µTBS),以及聚丙烯酸预处理对µTBS的影响。

材料与方法

在15颗第三磨牙上制备平坦的牙本质表面,随机分为5组:第1组 - RelyX ARC(对照组);第2组 - RelyX Unicem;第3组 - Maxcem Elite;第4组 - 22.5%聚丙烯酸与RelyX Unicem;第5组 - 22.5%聚丙烯酸与Maxcem Elite。在树脂水门汀上方构建一块复合树脂。将样本切片以获得梁状试件,每组20个试件在万能试验机上进行µTBS测试。通过扫描电子显微镜分析失效模式。

结果

根据方差分析和Tukey检验,RelyX ARC获得的µTBS均值最高(MPa)(21.38),与经聚丙烯酸预处理的Maxcem Elite(19.22)和经聚丙烯酸预处理的RelyX Unicem(17.75)在统计学上无差异(p>0.05)。后两组与RelyX Unicem(16.98)在统计学上无差异(p>0.05)。Maxcem Elite的均值最低(6.43),与其他组在统计学上有差异(p<0.05)。未经聚丙烯酸预处理的Maxcem Elite所有失效均为粘结性失效,其他组以混合性失效为主。

结论

与自粘树脂水门汀相比,RelyX ARC与牙本质的µTBS更高。聚丙烯酸预处理有效提高了Maxcem Elite的µTBS,但对RelyX Unicem的µTBS无影响。

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