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钎焊和激光焊接对陶瓷与金属之间结合强度的影响。

Effects of soldering and laser welding on bond strength of ceramic to metal.

机构信息

Department of Prosthodontics, School of Dentistry, University of Ege, Izmir, Turkey.

出版信息

J Prosthet Dent. 2011 Jan;105(1):28-34. doi: 10.1016/S0022-3913(10)60187-4.

Abstract

STATEMENT OF PROBLEM

Welding or soldering of metal frameworks negatively affects the overall bond strength between the veneering ceramic and metal.

PURPOSE

The purpose of this study was to evaluate the effect of soldering and laser-welding procedures on the bond strength between ceramic and metal.

MATERIAL AND METHODS

Thirty Ni-based metal specimens (Wiron 99) (8 × 4 × 4 mm) were fabricated and divided into 3 groups; soldered (S), laser welded (L), and control (untreated cast alloy) (n=10). In S and L specimens, a notch (1 × 1.5 mm) was prepared longitudinally on the surface of each specimen and filled with compatible alloy (Wiron soldering rods and Wiroweld NC, respectively). Vickers hardness measurements were made after polishing the surfaces with a metallographic polishing kit. A veneering ceramic (VITA VMK 95) was vibrated, condensed in a mold, and fired on the metal frameworks. The specimens were sectioned in 2 axes to obtain nontrimmed bar specimens with a bonding area of approximately 1 mm². Forty bars per block were obtained. Each bar was subjected to microtensile bond strength (μTBS) testing with a crosshead speed of 1 mm/min. The μTBS data (MPa) were recorded, and SEM was used for failure analysis of the tested bars. The measurements were statistically analyzed using a 1-way ANOVA and Tamhane tests (α=.05).

RESULTS

The mean differences in μTBS of veneering ceramic to soldered (10.4 ±2.4 MPa) and laser-welded (11.7 ±1.3 MPa) metal surfaces were not significantly different and were significantly lower than that of the cast alloy (25.4 ±3.6 MPa) (P<.05). The mean Vickers hardness of cast alloy was significantly higher (236 ±17 HV) than soldered (114 ±9 HV) and laser-welded groups (129 ±11 HV) (P<.05).

CONCLUSIONS

Soldering and laser welding significantly decreased the μTBS of a veneering ceramic to a base metal alloy.

摘要

问题陈述

金属框架的焊接或钎焊会对包埋陶瓷与金属之间的整体结合强度产生负面影响。

目的

本研究旨在评估钎焊和激光焊接程序对陶瓷与金属之间结合强度的影响。

材料和方法

制备了 30 个镍基金属试件(Wiron 99)(8×4×4mm),并分为 3 组;钎焊组(S)、激光焊接组(L)和对照组(未经处理的铸造合金)(n=10)。在 S 和 L 试件中,在每个试件的表面纵向制备一个 1×1.5mm 的缺口,并分别用相容合金(Wiron 钎料棒和 Wiroweld NC)填充。用金相抛光套件抛光表面后,进行维氏硬度测量。将包埋陶瓷(VITA VMK 95)振动、在模具中压实并在金属框架上烧结。将试件在 2 个轴上切割,获得约 1mm²结合面积的未修剪棒状试件。每个块获得 40 个棒。每个棒以 1mm/min 的十字头速度进行微拉伸结合强度(μTBS)测试。记录 μTBS 数据(MPa),并用 SEM 对测试棒的失效进行分析。使用单因素方差分析和 Tamhane 检验(α=.05)对测量值进行统计学分析。

结果

包埋陶瓷与钎焊(10.4±2.4MPa)和激光焊接(11.7±1.3MPa)金属表面的 μTBS 平均值差异无统计学意义,且显著低于铸造合金(25.4±3.6MPa)(P<.05)。铸造合金的平均维氏硬度显著高于钎焊组(114±9HV)和激光焊接组(129±11HV)(P<.05)。

结论

钎焊和激光焊接显著降低了包埋陶瓷与基底金属合金的 μTBS。

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