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4-[(3-Formyl-4-hydroxy-phen-yl)diazen-yl]-N-(pyrimidin-2-yl)benzene-sulfonamide.

作者信息

El-Ghamry Hoda, Issa Raafat, El-Baradie Kamal, Isagai Keiko, Masaoka Shigeyuki, Sakai Ken

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Aug 6;64(Pt 9):o1673-4. doi: 10.1107/S1600536808024239.

DOI:10.1107/S1600536808024239
PMID:21201664
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2960714/
Abstract

The title mol-ecule, C(17)H(13)N(5)O(4)S, has a trans configuration with respect to the diazenyl (azo) group. The pyrimidine ring and the terminal benzene ring are inclined at angles of 89.38 (4) and 1.6 (6)°, respectively, with respect to the central benzene ring. The conformation of the mol-ecule is in part stabilized by an intra-molecular O-H⋯O hydrogen bond. In the crystal structure, mol-ecules related through inversion centers form hydrogen-bonded dimers involving the sulfon-amide N-H group and the N atom of the pyrimidine ring.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/939b/2960714/e3c16f3b5ac6/e-64-o1673-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/939b/2960714/c84173e16184/e-64-o1673-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/939b/2960714/e3c16f3b5ac6/e-64-o1673-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/939b/2960714/c84173e16184/e-64-o1673-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/939b/2960714/e3c16f3b5ac6/e-64-o1673-fig2.jpg

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