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本文引用的文献

1
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
2
Modular chemistry: secondary building units as a basis for the design of highly porous and robust metal-organic carboxylate frameworks.
Acc Chem Res. 2001 Apr;34(4):319-30. doi: 10.1021/ar000034b.

聚[[二水合-三[μ(4)-(对苯二氧基)二乙酸根合]二镝(III)]]二水合物

Poly[[diaqua-tris[μ(4)-(p-phenyl-enedi-oxy)diacetato]didysprosium(III)] dihydrate].

作者信息

Li Ya-Feng, Wang Dao-Wu, Wang Yuan-Rui, Zhang Long

机构信息

School of Chemical Engineering, Changchun University of Technology, Changchun 130012, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Jun 19;64(Pt 7):m944. doi: 10.1107/S1600536808017649.

DOI:10.1107/S1600536808017649
PMID:21202796
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2961875/
Abstract

The title dysprosium coordination polymer, {[Dy(2)(C(10)H(8)O(6))(3)(H(2)O)(2)]·2H(2)O}(n), was synthesized by reacting dysprosium(III) nitrate and the flexible ligand (p-phenyl-enedi-oxy)diacetic acid under hydro-thermal conditions. Each Dy(III) ion is coordinated by nine O atoms in a tricapped trigonal prismatic geometry. The DyO(9) polyhedra form layers parallel to the bc plane. The rigid benzene rings of the anions link the layers along the a axis, forming a three-dimensional framework.

摘要

标题为镝配位聚合物{[Dy(2)(C(10)H(8)O(6))(3)(H(2)O)(2)]·2H(2)O}(n)，是通过硝酸镝(III)与柔性配体对苯二氧二乙酸在水热条件下反应合成的。每个Dy(III)离子由九个O原子以三帽三棱柱几何构型配位。DyO(9)多面体形成平行于bc平面的层。阴离子的刚性苯环沿a轴连接这些层，形成三维框架。